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Fractal bubble configuration controllable type slurry bed reactor

A reactor, controllable technology, applied in chemical instruments and methods, hydrocarbon oil cracking, hydrocarbon oil treatment, etc., can solve the problems of insufficient mixing intensity of the flow field in the reactor and inaccurate control of the bubble size. The effect of heat extraction and mass transfer, strong liquid turbulence, and uniform gas-liquid flow

Pending Publication Date: 2019-09-24
EAST CHINA UNIV OF SCI & TECH +2
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The purpose of this invention is to propose a strong mixing slurry with adjustable bubble configuration for enhanced heat transfer and mass transfer in view of the current situation that the bubble size control is inaccurate and the mixing intensity of the flow field inside the reactor is not enough in the current slurry bed reactor. bed reactor

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  • Fractal bubble configuration controllable type slurry bed reactor
  • Fractal bubble configuration controllable type slurry bed reactor
  • Fractal bubble configuration controllable type slurry bed reactor

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Embodiment Construction

[0028] At present, there are two main forms of slurry-bed gas distributors at home and abroad. One is that the gas phase enters the slurry-bed reactor through throttling bubbling; the other is that the gas phase enters the slurry-bed reactor after the liquid is sheared and broken. When the gas phase enters the slurry-bed reactor through the liquid shearing nozzle, the bubble size is difficult to control when the gas-liquid flow fluctuates or the process is adjusted, and the problems of flying temperature, coking, and product quality degradation are extremely easy to occur. However, the size of the bubbles generated by bubbling alone is too large to meet the increasingly refined reactor operating conditions. Using the A-type strong mixing method, both smaller bubbles and larger bubbles are produced, and the ratio of the two bubbles produced by this method is only related to the liquid phase flow rate, that is, under the same liquid phase feed, change into the reactor The gas rat...

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Abstract

The invention relates to a fractal bubble configuration controllable type slurry bed reactor, and belongs to a gas-liquid reactor device. The bubble controllable strong mixing is conducted at different reactor heights. According to a strong mixing internal part, a plurality of A-type strong mixing components are evenly distributed on a supporting partition plate of the reactor, and an M-type distribution component is arranged on the upper side of each A-type strong mixing component. Each A-type strong mixing component comprises a liquid phase lifting pipe, a gas phase lifting pipe, a short connection transverse pipe and a tail end nozzle, wherein liquid in the liquid phase lifting pipe is mixed with gas from the gas phase lifting pipe and the short connection transverse pipe, the mixture enters the tail end nozzle to release nitrogen bubbles of multiple dimensions, and the local liquid phase jet flow is formed above the partition plate. According to the slurry bed reactor, small bubbles are generated in throat pipes of the liquid phase lifting pipes through liquid phase entrainment, large bubbles are formed in the tail end nozzles through curved surface nozzle shearing, the gas-liquid flowing is even, the gas-liquid level below the partition plate is stable, the bubbles formed above the partition plate are controllable in dimensional, the liquid phase turbulence is strong, and the heat removal and mass transfer of the slurry bed reactor are facilitated.

Description

Technical field [0001] The invention relates to bubble reactor equipment, especially for the fields of hydrocracking and hydrorefining of inferior residual oil. The bubble size is adjustable under fluctuating conditions of high temperature and high pressure reactors, and a fractal bubble configuration that meets actual industrial applications Controllable slurry bed reactor. Background technique [0002] Slurry bed reactors are widely used in three-phase reactions such as coal-to-liquid Fischer-Tropsch synthesis reactions and residual oil hydrogenation. These reactions exotherm strongly and require heat to be taken inside the reactor. In addition, the diameter of the slurry-bed reactor can be up to 5 meters. In the process of reactor amplification, uneven temperature distribution often occurs, resulting in excessive local temperature rise, carbon deposition or deactivation of the catalyst, and decreased reaction selectivity. Consequences affect the amplification effect. Therefor...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J8/22C10G45/16C10G47/26
CPCB01J8/22B01J8/1872C10G45/16C10G47/26C10G2300/205C10G2300/202
Inventor 许萧杨强杨健刘凯祥宋智博万锦章徐松张小宁
Owner EAST CHINA UNIV OF SCI & TECH
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