Mixed negative electrode material, negative pole piece and preparation method thereof
A technology of negative electrode materials and negative electrode sheets, which is applied in the field of battery materials, can solve problems such as difficult control and complex process of mixed negative electrode materials, and achieve the effects of easy production control, high compaction density and long cycle life
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[0017] A third aspect of the present invention provides a method for preparing a negative electrode sheet, wherein the preparation method includes the following steps:
[0018] (1) the first carrier and the second carrier are physically mixed to obtain the mixed negative electrode material of the present invention;
[0019] (2) The mixed negative electrode material is mixed with a conductive agent and a binding agent, and the resulting mixed material is coated on the current collector.
[0020] In the present invention, in step (1), the physical mixing method is not particularly limited, as long as the first carrier and the second carrier can be mixed evenly, for example, the physical mixing can be done in a ball mill, a mixer or in a three-dimensional mixer.
[0021] In the present invention, the time of the physical mixing can be selected according to the mixing effect, as long as the materials are mixed uniformly within a certain period of time, preferably, the time of the...
Embodiment 1
[0032] (1) 440g of graphite with a median particle size of 10 μm and 440g of soft carbon with a median particle size of 10 μm were stirred and mixed by a stirrer for 2h to obtain a mixed negative electrode material;
[0033] (2) Stir and disperse the mixture of 1000g nitrogen methyl pyrrolidone solvent and 30g PVDF binder to obtain glue;
[0034] (3) 90g carbon black is uniformly mixed with the above-mentioned glue solution to obtain slurry A (viscosity is 5000cp);
[0035] (4) Add the mixed negative electrode material that step (1) obtains in the slurry A, and obtain the slurry B by mixing;
[0036] (5) Coat the slurry B on an aluminum foil (thickness: 12 μm, the same below), the formed coating is 65 μm, and dry at 115°C to obtain a negative electrode sheet.
Embodiment 2
[0038] (1) 560g of graphite with a median particle size of 1 μm and 240g of soft carbon with a median particle size of 20 μm were stirred and mixed by a stirrer for 1h to obtain a mixed negative electrode material;
[0039] (2) Stir and disperse the mixture of 1000g nitrogen methyl pyrrolidone solvent and 50g PVDF binder to obtain glue;
[0040] (3) 150g carbon black is uniformly mixed with the above-mentioned glue solution to obtain slurry A (viscosity is 10000cp);
[0041] (4) Add the mixed negative electrode material that step (1) obtains in the slurry A, and obtain the slurry B by mixing;
[0042] (5) Coat the slurry B on the aluminum foil to form a coating with a thickness of 100 μm, and dry it at 150° C. to obtain a negative electrode sheet.
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