Ideal two-dimensional Fermi liquid system Bi2O2Se single crystal and preparation method and application thereof
A single crystal and multi-purpose technology, applied in the ideal two-dimensional Fermi liquid system—Bi2O2Se single crystal and its preparation field, can solve the problem of small amount of crystal materials, achieve low cost, simple preparation method, and excellent crystal quality.
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Embodiment 2
[0062] Example 2. With Bi 2 o 3 , Bi, Se as raw materials through solidification and crystallization growth to obtain Bi 2 o 2 Se crystal
[0063] Weigh 0.01mol of Bi 2 o 3Powder (4.6608g), 0.01mol of Bi powder (2.0900g), and 0.015mol of Se powder (1.1845g) were mixed evenly and loaded into a pre-prepared quartz tube (length 10cm, diameter 2cm). Using a mechanical pump, The molecular pump is vacuumed and sealed, and then the sealed quartz tube is fixed on the pulling rod of the molten salt pulling furnace, and the raw material reaction temperature is set at 550°C, and the reaction time is 48h, and then the temperature is raised to 950°C, at 950°C Keep it warm for 24 hours to make it melt evenly, then cool down at a rate of 2°C / h. After a 10-day growth cycle, naturally cool down to obtain Bi 2 o 2 Se bulk, dissociated to obtain millimeter-scale Bi with high quality 2 o 2 Se single crystal, the maximum size reaches about 2mm, such as figure 2 (a) shown.
[0064] Such...
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