Vacuum cavity assembly for scattering experiment station

A technology of vacuum cavity and experimental station, which is applied in the direction of material analysis using radiation diffraction, material analysis using wave/particle radiation, and measuring devices, which can solve the problems of not being able to meet the experimental requirements at the same time, and achieve simple structure and easy maintenance Effect

Pending Publication Date: 2019-12-13
SHANGHAI INST OF APPLIED PHYSICS - CHINESE ACAD OF SCI
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Problems solved by technology

[0004] The purpose of the present invention is to provide a vacuum chamber assembly for a scattering experiment station, so as to solve the problem that the vacuum chamber in the prior art cannot meet the requirements of the three experimental methods of the small-angle scattering experiment station SAXS, GISAXS and low-resolution XRR at the same time. asked questions

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  • Vacuum cavity assembly for scattering experiment station

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Embodiment Construction

[0022] The present invention will be further described below in conjunction with specific embodiments. It should be understood that the following examples are only used to illustrate the present invention but not to limit the scope of the present invention.

[0023] Such as figure 1 Shown is a vacuum chamber assembly 100 for a scattering experiment station according to a preferred embodiment of the present invention, comprising: a vacuum chamber body 1 having a receiving space; Tube 2, one end of the bellows 2 is connected to the front end of the vacuum chamber body 1 through a vacuum flange, and the other end is connected to the vacuum pipeline (not shown in the figure); the light-transmitting window 3 arranged at the rear end of the vacuum chamber body 1 is preferably Large-diameter light-transmitting window, the polyimide film 4 is fixed at 3 places of the light-transmitting window by flanges and sealing rings, and is used to maintain the vacuum degree of the vacuum chambe...

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Abstract

The invention provides a vacuum cavity assembly for a scattering experiment station. The vacuum cavity assembly comprises a vacuum cavity body, a corrugated pipe connected to the front end of the vacuum cavity body, a light-transmitting window arranged at the rear end of the vacuum cavity body, two sets of two-dimensional motion platforms arranged at the bottom of the vacuum cavity assembly, a first beam stopper, a second beam stopper, and photodiodes; a polyimide film is fixed at the light-transmitting window; the first beam stopper and the second beam stopper are respectively connected withthe two-dimensional motion platforms through a connecting device; the photodiodes are respectively arranged on the first beam stopper and the second beam stopper and are used for measuring light intensity; and the first beam blocker and the second beam blocker can move simultaneously or separately, and meet the requirements of three kinds of experiments, namely, SAXS (small-angle X-ray scattering)experiments, GISAXS (grazing incidence small-angle X-ray scattering) experiments and low-resolution XRR (X-ray reflectivity) experiments at the same time. The vacuum cavity assembly can realize largeq value measurement of a sample, and is simple in structure and easy to maintain. The beam stoppers can be flexibly disassembled, so that different experiment requirements of different users are met;and hardware conditions are provided for the automatic sample matching of the GISAXS experiment of the experiment station.

Description

technical field [0001] The invention relates to the field of vacuum chamber devices, in particular to a vacuum chamber assembly for a scattering experiment station. Background technique [0002] The grazing incidence small-angle X-ray experimental technique is an experimental method for testing thin film samples. During the test, X-rays are incident on the surface of the sample at a certain grazing incidence angle, and the penetration depth of X-rays is adjusted by adjusting the grazing incidence angle to study the sample. Distribution of structures at different depths on the surface or surface layer. The grazing incidence small-angle X-ray experimental technique can be used to test the density, thickness, roughness, crystallite size and grain orientation of thin film samples. In the grazing incidence experiment, the X-rays passing through the sample are reflected and refracted on the surface of the sample, and the refracted light enters the interior of the sample, and is r...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N23/20008G01N23/201G01N23/20
CPCG01N23/20G01N23/20008G01N23/20075G01N23/201
Inventor 洪春霞王玉柱滑文强周平李秀宏边风刚
Owner SHANGHAI INST OF APPLIED PHYSICS - CHINESE ACAD OF SCI
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