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Preparation Process of Rose Essential Oil

A technology for rose essential oil and preparation process, which is applied in the directions of essential oil/spice, fat production, etc., can solve problems such as low extraction rate of essential oil, and achieve the effects of simple operation, improved acquisition rate and low cost

Inactive Publication Date: 2020-01-10
高治伟
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The purpose of the present invention is to provide a preparation process of rose essential oil, which combines the heating reflux method with the distillation method, and solves the problem of low extraction rate of essential oil in the prior art

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0021] A kind of preparation technology of rose essential oil of the present invention, specifically implement according to the following steps:

[0022] Step 1, taking freshly picked rose petals, air-drying them naturally until the water content is less than 20%, to obtain dried roses, then crushing the dried roses to a particle size of 5-10 meshes, and then mixing the crushed dried roses with dipropylene glycol The mass ratio of 1:5-10 is mixed, and extracted by heating and refluxing to obtain the rose extract;

[0023] Step 2, add deionized water with 0.2 to 0.3 times the mass of fresh rose petals into the still, then add the rose extract obtained in step 1 into the still, directly pass steam into the still to raise the temperature to 95°C-98°C, The steam pressure is controlled at 0.05-0.08MPa, and then the steam is stopped and changed to an indirect heating method outside the inner shell of the still so that the temperature of the condensation port of the still is maintain...

Embodiment 1

[0029] A kind of preparation technology of rose essential oil, specifically implement according to the following steps:

[0030] Step 1, take freshly picked rose petals, air-dry them naturally until the water content is less than 20%, and make dried roses, then crush the dried roses to a particle size of 5 mesh, then mix the dried roses with dipropylene glycol by 1: The mass ratio of 5 is mixed, and extracted by heating and refluxing to obtain the rose extract;

[0031] Step 2, add deionized water of 0.2 times the mass of fresh rose petals into the still, then add the rose extract obtained in step 1 into the still, directly pass steam into the still to raise the temperature to 95°C, and control the steam pressure at 0.05 MPa, then stop steaming and change to an indirect heating method outside the inner shell of the still so that the temperature of the condensation port of the still is maintained at 25°C to obtain a mixture of rose oil and rose hydrosol and a distillation resid...

Embodiment 2

[0037] A kind of preparation technology of rose essential oil, specifically implement according to the following steps:

[0038] Step 1, take freshly picked rose petals, air-dry them naturally until the water content is less than 20%, and make dried roses, then crush the dried roses to a particle size of 10 mesh, then mix the dried roses with dipropylene glycol by 1: The mass ratio of 10 is mixed, and extracted by heating and refluxing to obtain the rose extract;

[0039] Step 2, add deionized water with 0.3 times the mass of fresh rose petals into the still, then add the rose extract obtained in step 1 into the still, directly pass steam into the still to raise the temperature to 98°C, and control the steam pressure at 0.08 MPa, then stop steaming and change to an indirect heating method outside the inner shell of the still so that the temperature of the condensation port of the still is maintained at 38°C to obtain a mixture of rose oil and rose hydrosol and a distillation r...

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Abstract

The invention discloses a preparation process of rose essential oil, which comprises the following steps of: adopting freshly picked rose petals, naturally air drying, then crushing, mixing with dipropylene glycol, and adopting heating reflux extraction to obtain rose extract; adding deionized water to that distillation kettle, adding rose extract to the distillation kettle, directly passing steaminto the distillation kettle to raise the temperature to a certain temperature, and then stopping passing steam and changing to use an indirect heating mode outside the inner shell of the distillation kettle to maintain the temperature of the condensation port of the distillation kettle to be constant, so as to obtain a mixture of rose oil and rose pure dew and distillation residues; continuouslyadding the mixture of pure rose dew into the distillation kettle for distillation until the mass ratio of the obtained rose oil to the mixture of pure rose dew added into the distillation kettle is 0.1-0.5:100000, and collecting the rose oil to prepare the obtained rose essential oil. The invention combines the heating reflux method with the distillation method to solve the problem of low extraction rate of essential oil in the prior art.

Description

technical field [0001] The invention belongs to the technical field of plant extraction methods, and relates to a preparation process of rose essential oil. Background technique [0002] Rose essential oil is a world-renowned high-grade concentrated essence, a boutique among essential oils, and an important and expensive raw material for making high-end and expensive perfumes. It is not only used to make beauty, skin care, hair care and other cosmetics, but also widely used in medicine and food . [0003] Rose essential oil can not only adjust female endocrine, nourish the uterus, relieve dysmenorrhea, improve frigidity and menopausal discomfort. Moreover, it also has a very good beauty and skin care effect. It can nourish the inside and outside to dilute spots, promote the decomposition of melanin, improve dry skin, restore skin elasticity, and let women have white, elastic and healthy skin. It is an aromatic essential oil suitable for women's health care. [0004] Existi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02
CPCC11B9/02C11B9/025C11B9/027C11B9/022
Inventor 高治伟
Owner 高治伟