Preparation method of chitosan preservative film
A technology of chitosan and plastic wrap, which is applied in the field of preparation of chitosan plastic wrap, can solve the problems of poor water resistance of plastic wrap, and achieve the effects of reduced water permeability, good biocompatibility, and long-term food preservation time
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[0022] Example 1
[0023] (1) Dissolve 0.05 mol of chitosan with a degree of deacetylation of 85% in 500 mL of 1% acetic acid solution, add 0.05 mol of arabinose while stirring, react at 80 ℃ for 3 h, and cool to room temperature , Get product A;
[0024] (2) Mix 40 g of product A, 5 g of palm oil, 1 g of alkyl polyglucoside, 5 g of gum arabic and 20 g of modified starch to form mixture B, and put it into the shearing and dispersing machine at a rate of 12000 r / min Speed shear dispersion for 20 min, then add 0.1 g of polydimethylsiloxane, degas under reduced pressure at 0.1 MPa for 1 h, and then stir at 300 r / min for 60 min to obtain product C;
[0025] (3) Product C is evenly coated on the acrylic board after natural cooling, and dried at 50 ℃ to form a film to obtain the product.
Example Embodiment
[0026] Example 2
[0027] (1) Dissolve 0.05 mol of chitosan with a degree of deacetylation of 85% in 200 mL of 2% acetic acid solution, add 0.1 mol of arabinose while stirring, react at 100 ℃ for 2 h, and cool to room temperature , Get product A;
[0028] (2) Mix 50 g of product A, 10 g of palm oil, 2 g of alkyl polyglucoside, 10 g of gum arabic and 15 g of modified starch to form mixture B, and put it into the shearing and dispersing machine at a rate of 16000 r / min Disperse at speed for 5 min, then add 0.3 g of polydimethylsiloxane, degas under reduced pressure at 0.1 MPa for 2 h, and then stir at 400 r / min for 40 min to obtain product C;
[0029] (3) Product C is evenly coated on acrylic board after natural cooling, and dried at 60 ℃ to form a film, then the product is obtained.
Example Embodiment
[0030] Example 3
[0031] (1) Dissolve 0.05 mol of chitosan with 92% deacetylation degree in 100 mL of 3% acetic acid solution, add 0.15 mol of arabinose while stirring, react at 120 ℃ for 1 h, and cool to room temperature , Get product A;
[0032] (2) Mix 60 g of product A, 15 g of palm oil, 3 g of alkyl polyglucoside, 8 g of gum arabic and 10 g of modified starch to form mixture B, and put it into the shearing dispersing machine at a rate of 14000 r / min Disperse at speed for 10 min, add 0.2 g of polydimethylsiloxane, degas under reduced pressure at 0.1 MPa for 1.5 h, and then stir at 600 r / min for 30 min to obtain product C;
[0033] (3) Product C is evenly coated on acrylic board after natural cooling, and dried at 55 ℃ to form a film, then the product is obtained.
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