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Infrared chalcogenide glass lens and preparation method thereof

A technology of chalcogenide glass and glass substrate, which is applied in the direction of optical components, optics, instruments, etc., can solve the problems of unsatisfactory waterproof performance of glass lenses, and achieve improved surface hardness and waterproof performance, high transmittance, and reduced wear effect

Inactive Publication Date: 2020-03-13
安徽光智科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

But the waterproof performance of this glass lens is still unsatisfactory

Method used

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  • Infrared chalcogenide glass lens and preparation method thereof
  • Infrared chalcogenide glass lens and preparation method thereof
  • Infrared chalcogenide glass lens and preparation method thereof

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preparation example Construction

[0029] The present invention also proposes a method for preparing infrared chalcogenide glass lenses, which is used to prepare the above-mentioned infrared chalcogenide glass lenses. The preparation method includes the following steps: firstly, the glass substrate is placed in a coating machine, and the coating machine is vacuumed 1. Baking and heating the glass substrate, ion-cleaning the glass substrate, vapor-depositing an MgO coating, a first Ge coating, a first ZnS coating, a second Ge coating, and a second ZnS coating on the surface of the glass substrate in sequence, When the temperature of the glass substrate drops to 50°C, a superhard waterproof layer is applied.

[0030] In some embodiments of the present invention, the ion source used for ion cleaning is a Kaufmann type ion source. In some embodiments of the present invention, the shielding gas used for ion cleaning is argon, and the flow rate of the shielding gas is: 5-60 sccm / min. In some embodiments of the prese...

Embodiment 1

[0033] The glass substrate material adopted in this embodiment is As 40 Se 60 , put the glass substrate to be coated in an evaporation coating machine, and vacuum the evaporation coating machine until the vacuum degree reaches 3.0×10 -3 After Pa, the glass substrate is baked and heated, the baked heating set temperature is 100°C, and the constant temperature baked heating time is 10min, then the Kaufmann ion source is turned on, and the glass substrate is cleaned by the argon ion source for 5min, and then MgO coating, the first Ge coating, the first ZnS coating, the second Ge coating, and the second ZnS coating are evaporated on the double-sided surface of the glass substrate in sequence. The film thickness of the MgO coating is 5nm, and the film thickness of the first Ge coating is The film thickness of the first ZnS coating layer is 234nm, the film thickness of the second Ge coating layer is 425nm, and the film thickness of the second ZnS coating layer is 1122nm, then turn ...

Embodiment 2

[0035] The glass substrate material that present embodiment adopts is Ge 10 As 40 Se 50 , put the glass substrate to be coated in an evaporation coating machine, and vacuum the evaporation coating machine until the vacuum degree reaches 3.0×10 -3After Pa, the glass substrate is baked and heated, the baked heating set temperature is 70°C, and the constant temperature baked heating time is 20min, then the Kaufmann ion source is turned on, and the glass substrate is cleaned by the argon ion source for 8min, and then MgO coating, the first Ge coating, the first ZnS coating, the second Ge coating, and the second ZnS coating are evaporated on the double-sided surface of the glass substrate in sequence. The film thickness of the MgO coating is 20nm, and the film thickness of the first Ge coating is The film thickness of the first ZnS coating layer is 155nm, the film thickness of the second Ge coating layer is 965nm, and the film thickness of the second ZnS coating layer is 1046nm, ...

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Abstract

The invention relates to an infrared chalcogenide glass lens which comprises a glass substrate and a surface film layer plated on the surface of the glass substrate. The surface film layer comprises an MgO plating layer, a first Ge plating layer, a first ZnS plating layer, a second Ge plating layer, a second ZnS plating layer and a super-hard waterproof layer which are sequentially arranged from inside to outside. According to the infrared chalcogenide glass lens and a preparation method thereof, the application of a super-hard waterproof medicine to the infrared chalcogenide glass lens is realized. Stains, oil fouling and dust can be hardly adhered to the infrared chalcogenide glass lens plated with the super-hard waterproof layer, and the infrared chalcogenide glass lens is very easy toclean, so that the abrasion of the lens is reduced, the surface hardness and the waterproof performance of the infrared chalcogenide glass lens are improved, and the transmittance of the infrared chalcogenide glass lens within the infrared wavelength range of 8-12 microns is high.

Description

technical field [0001] The invention relates to the field of preparation of infrared optical materials, in particular to an infrared chalcogenide glass lens and a preparation method thereof. Background technique [0002] Chalcogenide glass is a special glass material with excellent infrared transmission properties. Compared with single crystal germanium, zinc selenide, zinc sulfide and other crystalline infrared materials, it has the characteristics of low thermal difference coefficient, good optical uniformity, and easy preparation. , is regarded as the core lens material of a new generation of temperature adaptive infrared optical system, which can meet the supporting requirements of high-end infrared imaging systems such as precision guided weapons, warship navigation and vehicle night vision. However, the chalcogenide glass itself has low hardness and low strength, and poor ability to withstand the complex external environment. After being coated with ordinary infrared c...

Claims

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Application Information

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IPC IPC(8): G02B1/14G02B1/18
CPCG02B1/14G02B1/18
Inventor 尹士平朱刘刘克武郭晨光
Owner 安徽光智科技有限公司