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Multifunctional wide-range spectral measurement device for diamond press

A spectral measurement, multi-functional technology, applied in measurement devices, fluorescence/phosphorescence, material analysis by optical means, etc., can solve the problems of poor signal-to-noise ratio, inability to take into account the fluorescence spectrum, difficult to achieve accurate measurement, etc., to achieve work performance The effect of stability, high measurement sensitivity, and strong functional integration

Pending Publication Date: 2020-03-17
CENT FOR HIGH PRESSURE SCI & TECH ADVANCED RES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The existing micro-spectroscopy system cannot realize the multi-functional in-situ spectral measurement under the diamond press. The main problems are: the reflection of light by multiple interfaces in the diamond press makes the signal-to-noise ratio of the measurement spectrum poor, and it is difficult to achieve accurate measurement ;The commonly used transmission objective lens cannot realize wide-spectrum data acquisition; the working distance of the objective lens is not enough, and the minimum working distance required by the diamond press is 16mm; and it cannot take into account the fluorescence spectrum, absorption spectrum, reflection spectrum, and optical path design for fluorescence imaging and spectrum acquisition

Method used

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  • Multifunctional wide-range spectral measurement device for diamond press
  • Multifunctional wide-range spectral measurement device for diamond press

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Effect test

Embodiment 1

[0024] This embodiment provides a multifunctional wide-range spectral measurement device for diamond presses, such as figure 1 shown, including:

[0025] The incident light source part, the laser incident part, the signal receiving part, and the microscopic optical path part; the transmitted incident light source part includes a lens 17, an optical fiber 18, and a light source 19; the microscopic optical path part includes: a first optical path switcher DPS 10, The second optical path switcher DPS-X 3, fluorescent illuminator 6, objective lens group 7, stage 9, first reflector 16, and fiber optic light source; the laser incident part includes 360nm channel 20, 660nm channel 21 and reserved In the laser router 1 of channel 22, the laser light is reflected by mirrors 23, 24, and 25, and then enters the dichroic filter in the second optical path switcher DPS-X 3 through the incident climbing frame and mirror 2, and passes through the dichroic filter in the second optical path swi...

Embodiment 2

[0037] This embodiment provides a multifunctional wide-range spectral measurement device for diamond presses, such as figure 2 As shown, including: color camera 31, plug-in filter set 32, two-speed DPS 33, lens barrel 34, camera 35, CMS36, fiber optic spectrometer 37, reflector 38, reflector 39, laser router 40, 325nm helium cadmium Laser 41, 355nm solid-state laser 42, 405nm solid-state laser 43, third gear DPS 44, fluorescence illumination module 45, objective lens group 46, sample 47, sample holder 48, mirror 49, lens 50, optical fiber 51, and light source 52.

[0038]The laser router 40 realizes the non-switching beam combination of various laser beams, and has built-in 325nm and 355nm long-pass dichroic chips and UV-enhanced aluminum mirrors. 325nm helium-cadmium laser 41 spot output diameter is 1.2mm, spatial light output power is 25mW; 355nm solid-state laser 42 spot output diameter is 2mm, space light output power is 10mW; 405nm solid-state laser 43 space light output...

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Abstract

The invention relates to a multifunctional wide-range spectral measurement device for a diamond press. The multifunctional wide-range spectral measurement device comprises a transmission incident light source part, a laser incident part, a signal receiving part and a microscopic light path part, wherein the microscopic light path part comprises a first light path switcher, a second light path switcher, fluorescent lighting equipment, an objective lens group, an objective table and a first reflecting mirror; the laser incident part comprises a laser router; the signal receiving part comprises athird light path switcher and at least one spectrograph, and is used for collecting an absorption spectrum, a reflection spectrum, a fluorescence spectrum and an image; and the first light path switcher is connected with the signal receiving part, the second light path switcher is connected with the laser incident part, and the first reflecting mirror is connected with the transmission incident light source part. The multifunctional wide-range spectral measurement device solves the technical problem that the fluorescence spectrum, the fluorescence imaging, the absorption spectrum and the reflection spectrum of a sample in the diamond press under high pressure are difficult to measure at the same time by means of an existing testing device, and realizes integrated in-situ measurement of the sample in the diamond press.

Description

technical field [0001] The invention relates to a spectrum measuring device, in particular to a multifunctional wide-range spectrum measuring device for a diamond press. Background technique [0002] High pressure is a controllable extreme condition widely used in the research of material science. When a substance is compressed under high pressure, its physical and chemical properties will change, and it can also form or transform into new structures and new materials that have not yet been recognized. High-pressure technology and its in-situ characterization provide new means and possibilities for natural science research. A diamond press, also called a diamond counter-anvil, is the most commonly used and effective device that can provide a high-pressure environment and realize in-situ characterization. The sample is sealed in a sealed cavity formed by two diamonds and a gasket. [0003] The existing micro-spectroscopy system cannot realize the multi-functional in-situ sp...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/64G01N21/01
CPCG01N21/6402G01N21/01
Inventor 吕旭杰郭嵩蒿殷海玮洪少欣
Owner CENT FOR HIGH PRESSURE SCI & TECH ADVANCED RES
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