High-density aquaculture sewage purification material and viscose-based activated carbon fiber loaded with purification material
An activated carbon fiber and aquaculture technology, applied in water/sewage treatment, water/sludge/sewage treatment, chemical instruments and methods, etc., can solve problems such as environmental damage and unfavorable sustainable development of high-density aquaculture, and achieve strong Purification ability, the effect of excellent purification ability
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Embodiment 1
[0026] The preparation of embodiment 1 high-density aquaculture sewage purification material
[0027] (1) Mix bentonite and sepiolite at a mass ratio of 1:1, soak in concentrated nitric acid for 12 hours, then wash with water until neutral to obtain a bentonite-sepiolite mixture;
[0028] (2) Mix oil (tung oil) with melamine, trehalose and surfactant (disodium ethanol lauryl sulfosuccinate monoester) in a mass ratio of 25:4:4:2 to obtain a mixture of oils;
[0029] (3) add bentonite-sepiolite mixture and grease mixture in organic solvent (select ethanol for use), after stirring evenly, concentrate and remove organic solvent, obtain bentonite-sepiolite-grease mixture; wherein organic solvent, bentonite-sepiolite mixture And the dosage ratio of the oil mixture is 25mL: 1g: 1g;
[0030] (4) Put the mixture of bentonite-sepiolite-grease under the protection of nitrogen; raise the temperature to 450°C at a heating rate of 4°C / min, keep it for 1.5h, then raise the temperature to 10...
Embodiment 2
[0031] Embodiment 2 Preparation of high-density aquaculture sewage purification material
[0032] (1) Mix bentonite and sepiolite in a mass ratio of 1:3, soak in concentrated nitric acid for 8 hours, and then wash with water until neutral to obtain a bentonite-sepiolite mixture;
[0033] (2) Mix oil (tung oil) with melamine, trehalose and surfactant (disodium ethanol lauryl sulfosuccinate monoester) in a mass ratio of 20:3:3:1 to obtain a mixture of oils;
[0034] (3) add bentonite-sepiolite mixture and grease mixture in organic solvent (select ethanol for use), after stirring evenly, concentrate and remove organic solvent, obtain bentonite-sepiolite-grease mixture; wherein organic solvent, bentonite-sepiolite mixture And the dosage ratio of the oil mixture is 20mL: 3g: 1g;
[0035] (4) Put the mixture of bentonite-sepiolite-grease under nitrogen protection; raise the temperature to 500°C at a heating rate of 5°C / min, keep it warm for 1h, then raise the temperature to 1100°C ...
Embodiment 3
[0036] Embodiment 3 Preparation of high-density aquaculture sewage purification material
[0037] (1) Mix bentonite and sepiolite in a mass ratio of 3:1, soak in concentrated nitric acid for 15 hours, then wash with water until neutral to obtain a bentonite-sepiolite mixture;
[0038] (2) Mix oil (tung oil) with melamine, trehalose and surfactant (disodium ethanol lauryl sulfosuccinate monoester) in a mass ratio of 30:5:5:3 to obtain a mixture of oils;
[0039] (3) add bentonite-sepiolite mixture and grease mixture in organic solvent (select ethanol for use), after stirring evenly, concentrate and remove organic solvent, obtain bentonite-sepiolite-grease mixture; wherein organic solvent, bentonite-sepiolite mixture And the dosage ratio of the oil mixture is 30mL: 1g: 3g;
[0040] (4) Put the bentonite-sepiolite-grease mixture under the protection of nitrogen; raise the temperature to 400°C at a heating rate of 3°C / min, keep it warm for 2h, then raise the temperature to 900°C ...
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