Endolysosomal targeting conjugates for improved delivery of cargo molecules to the endolysosomal compartment of target cells
A technology of endolysosomes and conjugates, applied in the direction of radioactive carriers, preparations for in vivo tests, antibodies, etc.
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Embodiment 1
[0213] Example 1. Materials and methods
[0214] Cell lines and culture conditions. The mouse endothelial cell line 2H11 (ATCC, CRL-2163) was cultured in Darwin's Modified Elder's Medium (DMEM) supplemented with 5% heat-inactivated fetal bovine serum (FBS). Human breast cancer cell line MDA-MB-231 (ATCC, HTB-26) was cultured in DMEM supplemented with 10% FBS. Human breast cancer cell lines T-47D (ATCC, HTB-133), MDA-MB-453 (ATCC, HTB-131) and MDA-MB-468 (ATCC, HTB-132) were prepared in RPMI 1640 supplemented with 10% FBS cultured in culture medium. Human breast cancer cell line SK-BR-3 (ATCC, HTB-30) and human ovarian cancer cell line SK-OV-3 (ATCC, HTB-77) were cultured in McCoy's 5A medium supplemented with 10% FBS. Human prostate cancer cell lines LNCaP and 22Rv1 (ATCC, CRL-1740 and CRL-2505, respectively) were cultured in RPMI 1640 medium supplemented with 10% FBS. Human breast cancer cell line HCC1954 (Gazdar, A.F., Kurvari, V., Virmani, A., Gollahon, L., Sakaguchi...
Embodiment 2
[0247] Example 2. Generation of HER2 targeting agents with pH dependent HER2 binding
[0248] Figure 4A and 4B Binding assays showing two mutated Pertuzumab variants targeting HER2: SG mutant; Ser55 mutated to histidine and Gly57 mutated to glutamic acid in the heavy chain variable domain (SEQ ID NO: 4 ); YS mutant, Tyr55 in the light chain variable domain is mutated to histidine, and Ser103 in the heavy chain variable domain is mutated to histidine (SEQ ID NO:6,8). Data were acquired using surface plasmon resonance. Figure 4A Representative sensorgrams at pH 7.0 and 5.8, 1 μM HER-extracellular domain (ECD)-Fc fusion interaction with mutant variants and wild-type (WT) Pertuzumab are shown. for Figure 4A For the assay shown in , antibodies were immobilized on the flow cell. Figure 4B Equilibrium dissociation constants (nM) of WT Pertuzumab, SG and YS obtained by injecting antibodies on immobilized HER2-ECD-Fc are shown. The data indicated that both the SG and YS var...
Embodiment 3
[0249] Example 3. Internalization and accumulation of HER2 targeting agents in HER2 expressing cells
[0250] Pertuzumab (WT) and mutant variants SG and YS were coupled to maleimidocaproyl-val-cit-PAB-MMAE (MC-VC-PAB -MMAE), a drug-to-antibody ratio (DAR) of 2 drugs per antibody, followed by analysis of binding and accumulation of HER2-targeted ADCs (HER2-ADCs) in a panel of different HER2-expressing cell lines. Figure 5A HER2 expression levels on different cancer cell lines detected using Alexa 647-labeled Pertuzumab (solid line) or Alexa 647-labeled control antibody (dashed line) and flow cytometry are shown. Figure 5B Shown are the internalized Alexa 488-labeled WT Pertuzumab-MMAE (WT-MMAE), SG-MMAE, YS-MMAE, control antibody-MMAE (C-MMAE) or Trg after 0.5, 4 and 20 hours of incubation. Tocilizumab-DM1 (T-DM1) levels. Cell surface-bound ADCs were quenched using an Alexa 488-specific antibody. Error bars indicate standard deviation, * indicates statistically significa...
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