Coupling light-emitting material and preparation method thereof

A technology of optical materials and raw materials, applied in the direction of luminescent materials, chemical instruments and methods, silicon organic compounds, etc., can solve the problems of inability to extract light, light loss, etc., and achieve enhanced planarity, increased refractive index, and increased thermal stability. Effect

Inactive Publication Date: 2020-04-03
WUHAN CHINA STAR OPTOELECTRONICS SEMICON DISPLAY TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Whether it is a bottom-emitting device or a top-emitting device, most of the electro-generated

Method used

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  • Coupling light-emitting material and preparation method thereof
  • Coupling light-emitting material and preparation method thereof
  • Coupling light-emitting material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] Synthesize the following target product-compound 1:

[0029]

[0030] The synthetic reaction formula is as follows:

[0031]

[0032] In the general structure formula, n=1,2;

[0033] m=0,1,2. Wherein, the specific structural formula of Ar in the general formula is as follows:

[0034] Preferably, at least one Ar in the general formula comprises any one or more of the following structures or derivatives 1-5 thereof:

[0035]

[0036] Preferably, other Ar in the general formula comprises any one or more of the following structures or derivatives 6-19 thereof:

[0037]

[0038]

[0039] In the above two general formulas, the structural formulas of Ar1-6 can be the same or different, at least one structural formula of Ar in the general formula can choose any structural formula in derivatives 1-5, Ar must choose the structural formula of derivatives 1-5; Other structural formulas of Ar may be any one of derivatives 6-19.

[0040] Based on the general s...

Embodiment 2

[0053] Synthesize the following target product-compound 2:

[0054]

[0055] The synthetic reaction formula of compound 2:

[0056]

[0057] In the general structure formula, n=1,2; m=0,1,2. Wherein, the specific structural formula of Ar in the general formula is as follows:

[0058] Preferably, at least one Ar in the general formula comprises any one or more of the following structures or derivatives 1-8 thereof:

[0059]

[0060] Other Ar in the general formula includes any one or more of the following structures or derivatives thereof:

[0061]

[0062]

[0063] In the above two general formulas, the structural formulas of Ar1-6 can be the same or different, at least one structural formula of Ar in the general formula can choose any structural formula in derivatives 1-8, Ar must choose the structural formula of derivatives 1-5; Other structural formulas of Ar may be optional. Derivatives may choose any structural formula in the second group.

[0064] Base...

Embodiment 3

[0078] Synthesize the following target product-compound 3:

[0079]

[0080] The synthetic reaction formula of compound 3:

[0081]

[0082] In the general structure formula, n=1,2; m=0,1,2. Wherein, the specific structural formula of Ar in the general formula is as follows:

[0083] Preferably, at least one Ar in the general formula comprises any one or more of the following structures or derivatives 1-5 thereof:

[0084]

[0085] Other Ar in the general formula includes any one or more of the following structures or derivatives thereof:

[0086]

[0087] Based on the general structural formula of the above-mentioned light-coupling material, through different raw materials, one or more of the following structural formulas can be synthesized:

[0088]

[0089]

[0090]

[0091] The present invention also provides a method for preparing a light-coupling material, which includes the following steps:

[0092] Step 1) Dissolve benzo[5,6][1,4]thiazolo[2,3...

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Abstract

The invention provides an improved coupling light-emitting material, and aims to obtain the coupling light-emitting material with high thermal stability and high refractive index. The structural general formula is disclosed in the invention, wherein n = 1, 2; m=0, 1, 2. A series of substituted aniline CPL based on thiazolo [2, 3, 4-kl] phenothiazine is synthesized. According to the molecules, benzene rings in triphenylamine are connected through carbon-sulfur bonds to form silane naphthalene [3, 2, 1-de] anthracene, so that substituted arylamine materials are synthesized. The rigidity and planarity of the material are enhanced, so that the CPL thermal stability is improved, the refractive index of the material is obviously improved, and coupling light emission is facilitated. The inventionalso provides a preparation method of the coupling light-emitting material.

Description

technical field [0001] The invention relates to the field of optoelectronic technology, in particular to a light-coupling material and a preparation method thereof. Background technique [0002] Organic light-emitting diodes (organic lighting-emitting diodes, OLEDs), due to active light emission, large viewing angle, fast response speed, wide temperature range, low driving voltage, low power consumption, high brightness, simple production process, light and thin, and can The advantages of flexible display have shown great application prospects in the fields of OLED display and lighting, attracting the attention of researchers and companies. [0003] Whether it is a bottom-emitting device or a top-emitting device, most of the electro-generated light is lost inside the device, and the generated light cannot be effectively taken out of the device. At present, the general solution is to coat an organic light coupling layer (CPL) on the outside of the device electrode to increas...

Claims

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Application Information

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IPC IPC(8): C07D455/03C07D471/16C07D498/06C07D513/06C07D513/16C07D519/00C07F7/08C09K11/06H01L51/54
CPCC07D498/06C07D513/06C07D513/16C07D455/03C07D471/16C07D519/00C09K11/06C07F7/0816C09K2211/1037C09K2211/1029C09K2211/1033C09K2211/104H10K85/636H10K85/631H10K85/657H10K85/40H10K85/6572
Inventor 王彦杰
Owner WUHAN CHINA STAR OPTOELECTRONICS SEMICON DISPLAY TECH CO LTD
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