Liquid expanding agent expanding step by step and preparation method thereof

A technology for liquid expansion and powder mixing, applied in the field of building materials, can solve the problems of shrinkage and cracking of concrete, large amount of finely ground fly ash and slag powder, and troublesome concrete, so as to avoid excessive expansion stress, The effect of slowing the expansion rate and controlling the rate of hydration

Active Publication Date: 2020-04-07
HUBEI UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, fiber-mixed concrete is cumbersome and costly, and the amount of finely ground fly ash and slag powder is large, which requires high cost and cannot completely solve the shrinkage and cracking of concrete.

Method used

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  • Liquid expanding agent expanding step by step and preparation method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 2

[0055] A method for preparing a step-by-step expansion liquid expansion agent, the total mass of raw materials is 100 parts, the solid content is about 10%, and it is mainly prepared from the following components:

[0056] 700 ℃ nano magnesium oxide powder: 1.0 parts

[0057] 900°C nano-magnesia powder: 0.8 parts

[0058] 1100°C nano-magnesia powder: 0.5 parts

[0059] Butanol: 0.2 parts

[0060] Simethicone oil: 0.3 parts

[0061] Span 80: 0.3 servings

[0062] Polypropylene alcohol 400: 0.6 parts

[0063] Lauryl polyoxyethylene ether: 2.6 parts

[0064] Propylene glycol methyl ether: 2.6 parts

[0065] Polyacrylamide: 1.2 parts

[0066] Step 1: Weigh 1.0 parts of 700°C nano-magnesia powder, 0.8 parts of 900°C nano-magnesia powder, 0.5 parts of 1100°C nano-magnesia powder, 0.2 parts of butanol, 0.3 parts of simethicone, and 0.3 parts of Si Place 80 parts of pan and 90 parts of water in the reaction kettle, control the temperature of the water bath at 40°C, and stir at...

Embodiment 3

[0070] A method for preparing a step-by-step expansion liquid expansion agent, the total mass of raw materials is 100 parts, the solid content is about 10%, and it is mainly prepared from the following components:

[0071] 700°C nano-magnesia powder: 1.4 parts

[0072] 900°C nano-magnesia powder: 0.8 parts

[0073] 1100°C nano-magnesia powder: 0.5 parts

[0074] Butanol: 0.3 parts

[0075] Simethicone oil: 0.2 parts

[0076] Span 80: 0.4 servings

[0077] Polypropylene alcohol 400: 0.7 parts

[0078] Lauryl polyoxyethylene ether: 2.5 parts

[0079] Propylene glycol methyl ether: 2.5 parts

[0080] Polyacrylamide: 1.0 parts

[0081] Step 1: Weigh 1.4 parts of 700°C nano-magnesia powder, 0.8 parts of 900°C nano-magnesia powder, 0.5 parts of 1100°C nano-magnesia powder, 0.3 parts of butanol, 0.2 parts of simethicone, 0.4 parts of Si Place 80 parts of pan and 90 parts of water in the reaction kettle, control the temperature of the water bath at 35°C, and stir at constant t...

Embodiment 4

[0085] A method for preparing a step-by-step expansion liquid expansion agent, the total mass of raw materials is 100 parts, the solid content is about 10%, and it is mainly prepared from the following components:

[0086] 700 ℃ nano magnesium oxide powder: 1.3 parts

[0087] 900°C nano-magnesia powder: 0.9 parts

[0088] 1100°C nano-magnesia powder: 0.8 parts

[0089] Butanol: 0.3 parts

[0090] Simethicone oil: 0.2 parts

[0091] Span 80: 0.4 servings

[0092] Polypropylene alcohol 400: 0.8 parts

[0093] Lauryl polyoxyethylene ether: 2.4 parts

[0094] Propylene glycol methyl ether: 2.4 parts

[0095] Polyacrylamide: 0.8 parts

[0096] Step 1: Weigh 1.3 parts of 700°C nano-magnesia powder, 0.9 parts of 900°C nano-magnesia powder, 0.8 parts of 1100°C nano-magnesia powder, 0.3 parts of butanol, 0.2 parts of simethicone, 0.4 parts of Si Place 80 parts of the pan and 90 parts of water in the reaction kettle, control the temperature of the water bath at 30°C, and stir at...

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Abstract

The invention discloses a liquid expanding agent capable of expanding step by step and a preparation method thereof. The liquid expanding agent is prepared by the following steps: 1, weighing a nano magnesium oxide powder mixture, butanol, span-80 and water, and stirring at a constant temperature of 30-40 DEG C for 1 hour; 2, heating to 50-70 DEG C, sequentially adding polypropylene glycol 400, dimethicone and a shrinkage reducing component, and stirring for 1-2 hours; and 3, adding polyacrylamide, stirring for 1-2 hours, curing at constant temperature for 1 hour, and cooling to room temperature to obtain the liquid expanding agent capable of expanding step by step. An expansion component in the liquid expanding agent is formed by grinding, modifying and mixing magnesium oxide fired at different temperatures of 700 DEG C, 900 DEG C and 1100 DEG C, the magnesium oxide powder is mixed and ground to a nanometer level, the hydration time of the three magnesium oxide powder prepared at different firing temperatures is different, and the step-by-step expansion effect is achieved; by compounding with the shrinkage reducing component and the like, the volume expansion of concrete can be remarkably improved, the concrete volume shrinkage is reduced, and the crack resistance and impermeability of concrete are improved.

Description

technical field [0001] The invention belongs to the technical field of building materials, and relates to an expansion agent, in particular to a liquid expansion agent with a high expansion rate and a preparation method thereof. Background technique [0002] During the pouring and hardening process of cement-based cementitious materials, volume shrinkage will be caused by chemical shrinkage, cold shrinkage and dry shrinkage, and even cracking of the material will occur in severe cases. Add fiber, pulverized fly ash or slag powder and expansion agent into concrete to solve the shrinkage and cracking problems of concrete. However, fiber-mixed concrete is cumbersome and costly, and the amount of finely ground fly ash and slag powder is large, which requires high cost and cannot completely solve the shrinkage and cracking of concrete. However, expansion agent is a kind of chemical additive. When mixed into concrete, when the concrete sets and hardens, it expands and blocks capi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B24/42
CPCC04B40/0046C04B2103/0068C04B14/304C04B24/00C04B24/42C04B24/08C04B24/26C04B24/32C04B24/023C04B24/2652
Inventor 柯凯姚恒
Owner HUBEI UNIV OF TECH
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