Special magnetic pressure-sensitive adhesive for prism film
A prismatic film and pressure-sensitive adhesive technology, applied in the direction of adhesive types, adhesive additives, non-polymer adhesive additives, etc., can solve the problems of unreusable prismatic films, lack of adhesiveness of pressure-sensitive adhesives, waste, etc. , to achieve long-term magnetism, prevent oxidation, reduce the effect of agglomeration
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Embodiment 1
[0026] This embodiment relates to a special pressure-sensitive adhesive for prism film with magnetism, which specifically includes the following:
[0027] First, the preparation of modified magnetic particles is as follows:
[0028] (1) Mix polyethylene glycol and polyethylene glycol monomethyl ether in a flask at a mass ratio of 1:2, and add dichloromethane 30 times the mass of polyethylene glycol and 0.5 times the mass of polyethylene glycol to the flask After stirring and mixing, 2-bromopropionyl bromide with 0.2 times the mass of polyethylene glycol was added to the flask, and nitrogen gas was introduced into the flask at a rate of 35mL / min. After stirring and reacting under the conditions for 18 hours, concentrate by rotary evaporation, evaporate half of the solvent to obtain a concentrated solution, then precipitate the concentrated solution with ether, and filter to obtain a solid initiator;
[0029] (2) Mix the initiator obtained in step (1) and copper bromide in a th...
Embodiment 2
[0036]This embodiment relates to a special pressure-sensitive adhesive for prism film. On the basis of Embodiment 1, the ratio of raw materials is modified, as follows: in parts by weight, weigh in order: 90 parts of water-based acrylate emulsion, 6 parts of silane Coupling agent KH-570, 10 parts of modified magnetic particles, 26 parts of curing agent, 21 parts of water and 2 parts of emulsifier, mix water-based acrylic emulsion with silane coupling agent KH-570, and add water-based acrylic emulsion and Add modified magnetic particles to the mixture of silane coupling agent KH-570, stir and mix for 1 hour at a temperature of 40°C and a speed of 600r / min to obtain component A; mix the curing agent with water, and Add emulsifier to the mixture of emulsifier and water, and stir and mix for 80 minutes under the condition of temperature of 40°C and rotation speed of 600r / min to obtain component B. Separately package components A and B to obtain a magnetic prism Film special pressu...
Embodiment 3
[0038] This embodiment relates to a special pressure-sensitive adhesive for prism film. On the basis of Embodiment 1, the ratio of raw materials is modified, as follows: in parts by weight, weigh in order: 85 parts of water-based acrylate emulsion, 5 parts of silane Coupling agent KH-570, 9 parts of modified magnetic particles, 24 parts of curing agent, 18 parts of water and 3 parts of emulsifier, mix the water-based acrylic emulsion with silane coupling agent KH-570, and add water-based acrylic emulsion and Add modified magnetic particles to the mixture of silane coupling agent KH-570, stir and mix for 1 hour at a temperature of 40°C and a speed of 600r / min to obtain component A; mix the curing agent with water, and Add emulsifier to the mixture of emulsifier and water, and stir and mix for 80 minutes under the condition of temperature of 40°C and rotation speed of 600r / min to obtain component B. Separately package components A and B to obtain a magnetic prism Film special pr...
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