Control method of expansion coefficient of light weight dense near zero expansion metal matrix composites

A composite material and near-zero expansion technology, which is applied in the field of lightweight near-zero-expansion composite materials, can solve problems such as easy damage, inability to change the temperature range of low thermal expansion coefficient, and inability to realize a wide range of thermal expansion coefficient, etc. The method is simple and easy to implement, and the effect of good mechanical properties and electrical and thermal conductivity characteristics

Active Publication Date: 2021-09-21
SHANGHAI JIAOTONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the above-mentioned patent has the following disadvantages: patent 201611041751.3 cannot realize the adjustment of a wide range of thermal expansion coefficients, it is difficult to prepare a composite material with zero expansion, and patent 201611041751.3 cannot change the temperature range where the low thermal expansion coefficient occurs
Due to the characteristics of the material itself, the resin-based composite material has the disadvantages of brittleness, easy aging, non-temperature resistance, and easy damage, which greatly limits its application range.
However, there are no relevant reports at home and abroad on the research of metal matrix composites with light weight, near-zero expansion characteristics and metal properties.

Method used

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  • Control method of expansion coefficient of light weight dense near zero expansion metal matrix composites
  • Control method of expansion coefficient of light weight dense near zero expansion metal matrix composites
  • Control method of expansion coefficient of light weight dense near zero expansion metal matrix composites

Examples

Experimental program
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Effect test

Embodiment 1

[0031] refer to figure 1 As shown, it is a flow chart of a method for regulating the expansion coefficient of a light-weight dense near-zero-expansion metal matrix composite material according to an embodiment of the present invention. The figure includes the following steps:

[0032] Negative expansion material Mn 3 (Mn 0.1 Zn 0.5 sn 0.4 ) Preparation of N powder: the bulk negative expansion material Mn 3 (Mn 0.1 Zn 0.5 sn 0.4 )N is ground with a vacuum ball mill, and sieved to obtain a powder of 75-150 μm, and set aside.

[0033] Then the prepared negative expansion material Mn 3 (Mn 0.1 Zn 0.5 sn 0.4 )N powder and pure aluminum powder with a purity of 99.95% and a particle size of 25 μm are mixed according to the volume ratio of 2:8, 3:7, and 4:6 respectively. The mixing time is 30 hours, and the mixing speed is 150r / min. The first composite material mixed powder, the second composite material mixed powder and the third composite material mixed powder are respec...

Embodiment 2

[0038] refer to figure 1 As shown, it is a flow chart of a method for regulating the expansion coefficient of a light-weight dense near-zero-expansion metal matrix composite material according to an embodiment of the present invention. The figure includes the following steps:

[0039] Negative expansion material Mn 3 (Mn 0.1 Zn 0.5 sn 0.4 ) Preparation of N powder: the bulk negative expansion material Mn 3 (Mn 0.1 Zn 0.5 sn 0.4 )N is ground with a vacuum ball mill, and sieved to obtain a powder of 2-40 μm, and set aside.

[0040] Then the prepared negative expansion material Mn 3 (Mn 0.1 Zn 0.5 sn 0.4 )N powder and aluminum powder with a purity of 99.95% and a particle size of 25 μm were mixed according to a volume ratio of 3:7, the mixing time was 30 hours, and the mixing speed was 150 r / min to obtain a composite material mixing powder for later use.

[0041] Put the prepared composite material mixed powder into a vacuum hot-press sintering furnace for hot-press s...

Embodiment 3

[0044] refer to figure 1 As shown, it is a flow chart of a method for regulating the expansion coefficient of a light-weight dense near-zero-expansion metal matrix composite material according to an embodiment of the present invention. The figure includes the following steps:

[0045] Negative expansion material Mn 3 (Mn 0.1 Zn 0.5 sn 0.4 ) Preparation of N powder: the bulk negative expansion material Mn 3 (Mn 0.1 Zn 0.5 sn 0.4 )N is ground with a vacuum ball mill, and sieved to obtain a powder of 40-75 μm, and set aside.

[0046] Then the prepared negative expansion material Mn 3 (Mn 0.1 Zn 0.5 sn 0.4 )N powder and aluminum powder with a purity of 99.95% and a particle size of 25 μm were mixed according to a volume ratio of 3:7, the mixing time was 30 hours, and the mixing speed was 150 r / min to obtain a composite material mixing powder for later use.

[0047] Put the prepared composite material mixed powder into a vacuum hot-press sintering furnace for hot-press ...

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Abstract

The invention provides a method for controlling the expansion coefficient of a lightweight and dense near-zero expansion metal matrix composite material, comprising: using a negative expansion material Mn 3 (Mn x Zn y sn z )N powder and metal matrix powder are raw materials, and the metal matrix is ​​selected from any one of pure aluminum, pure copper, aluminum alloy, magnesium alloy, titanium alloy, and copper alloy; the negative expansion material Mn 3 (Mn x Zn y sn z ) N powder is mixed with the metal matrix powder to obtain a mixed powder; adjust the ratio of the negative expansion material powder and the metal matrix powder, and / or adjust the negative expansion material Mn 3 (Mn x Zn y sn z ) N powder particle size, to obtain light and dense near-zero expansion metal matrix composites; wherein: the negative expansion material powder accounts for 1-50% of the total volume of the metal matrix composite, and the metal matrix powder accounts for 1-50% of the total volume of the metal matrix composite. 99%‑50% of the total volume; negative expansion material Mn 3 (Mn x Zn y sn z ) The particle size of the N powder is adjusted within less than 150 μm. The present invention adjusts the negative expansion material Mn 3 (Mn x Zn y sn z ) N powder particle size and content, so as to realize the regulation of thermal expansion coefficient (including zero expansion) of various metal matrix composites.

Description

technical field [0001] The invention relates to a lightweight near-zero-expansion composite material, in particular to a method for adjusting the expansion coefficient of a light-weight dense near-zero-expansion metal-based composite material. Background technique [0002] Most materials in nature exhibit the phenomenon of "expanding with heat and contracting with cold". This characteristic of materials not only provides many conveniences to human beings, but also brings many troubles to modern life. The main reason is that thermal expansion and contraction will cause thermal stress inside the material, and even lead to cracks and failure of the material. The nature of a material's volume change with temperature can also have a major impact on the accuracy of precision parts. For example, for the precise light focusing and optical path alignment of precision optical equipment such as telescopes, laser equipment, and optical fiber communications, the "minimum loss" of the co...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C22C32/00C22C21/00C22C1/05B22F3/14C22C1/10
CPCB22F3/14C22C1/05C22C21/00C22C32/0068
Inventor 欧阳求保曹贺崔铎
Owner SHANGHAI JIAOTONG UNIV
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