Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Method for preparing cigarette filter capsule from lignin-carbohydrate coated essence

A carbohydrate and lignin technology, applied in the fields of tobacco, application, and tobacco treatment, can solve the problems of unreported natural rigid wrapping materials, insufficient brittleness, and weak popping feeling, etc.

Active Publication Date: 2020-04-24
HUBEI CHINA TOBACCO IND +1
View PDF7 Cites 4 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the technology of loading essence with popping beads is mainly based on adsorption, and the loading rate is not high; at the same time, the wrapping technology is also gradually emerging, but it is often prepared by wrapping essence with sodium alginate, and the feeling of bursting when squeezed is not strong, which is due to alginic acid. Sodium is a kind of flexible material, which is caused by insufficient brittleness.
However, natural rigid wrapping materials have not been reported

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for preparing cigarette filter capsule from lignin-carbohydrate coated essence

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A kind of lignin-carbohydrate-coated essence prepares the method for cracking pearls for cigarettes, comprising the following steps:

[0028] (1) Prepare castor oil as the oil phase, menthol as the essence, and choose spruce LCC.

[0029] The extraction method of spruce LCC is as follows: weigh a certain amount of dry spruce wood powder, wrap it in quantitative filter paper with a thin thread, put it in a Soxhlet extractor, add toluene / ethanol (2 / 1, v / v) , extracted in a water bath for 6h. The extracted spruce wood powder was placed in a ball mill for vibration milling for 64 hours. Put the ball-milled spruce wood powder in quantitative filter paper and wrap it with a thin thread, put it in a Soxhlet extractor, add dioxane / water (96 / 4, v / v), and extract it in an oil bath. Extracted for 72h to obtain solution and insoluble matter. After the insoluble matter is fully dried, add acetic acid / water (1 / 1, v / v) and extract for 24 hours to obtain the insoluble matter and sol...

Embodiment 2

[0036] A kind of lignin-carbohydrate-coated essence prepares the method for cracking pearls for cigarettes, comprising the following steps:

[0037] (1) Prepare peanut oil as the oil phase, menthol as the essence, and poplar LCC. The extraction method of Poplar LCC is as in Example 1.

[0038] (2) According to parts by mass, 0.6 part of oil-soluble essence solution was dissolved in 100 parts of oil phase to obtain oil phase solution; 1 part of lignin-carbohydrate complex was dissolved in 100 parts of water to obtain water phase solution.

[0039] (3) Mix the oil phase solution and the water phase solution at a volume ratio of 15:100; send them to a high-speed shearing machine after mixing, and shear at a high speed of 5000rpm for 2min; Quality, cycle 2 times to obtain emulsion system.

[0040] (4) Add 10 times the volume of anhydrous methanol drop by drop to the emulsion system, let it stand until the precipitation no longer increases, and then let it stand for 30 minutes to...

Embodiment 3

[0044] A kind of lignin-carbohydrate-coated essence prepares the method for cracking pearls for cigarettes, comprising the following steps:

[0045] (1) Prepare peanut oil as the oil phase, vanillin as the essence, and use wheat straw LCC. The extraction method of wheat straw LCC is as in Example 1.

[0046] (2) Dissolving 8 parts of oil-soluble essence solution in 100 parts of oil phase in parts by mass to obtain an oil phase solution; dissolving 8 parts of lignin-carbohydrate complex in 100 parts of water to obtain a water phase solution.

[0047](3) Mix the oil phase solution and the water phase solution at a volume ratio of 30:100; send them to a high-speed shearing machine after mixing, and shear at a high speed of 15,000 rpm for 8 minutes; Quality, cycled 3 times to obtain emulsion system.

[0048] (4) Add 100 times the volume of glycerol drop by drop to the emulsion system, let it stand until the precipitation no longer increases, and then let it stand for 60 minutes ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention relates to the technical field of cigarette filter capsules, in particular to a method for preparing a cigarette filter capsule from lignin-carbohydrate coated essence. The preparation method comprises the following steps of: preparing an oil phase solution: dissolving an oil-soluble essence solution into an oil phase; preparing an aqueous phase solution: dissolving a lignin-carbohydrate complex (LCC) in water; then mixing the oil phase solution with the aqueous phase solution to obtain an emulsion system; adding a reverse solvent dropwise into the emulsion system, and performingstanding to obtain microsphere precipitate; and filtering and drying the microsphere precipitate to obtain the cigarette filter capsule. An emulsion system is formed by utilizing LCC amphipathy and is employed to wrap oil-soluble essence, so that the load rate of the oil-soluble essence is increased, and also the subjective use feeling of the filter capsule is improved.

Description

technical field [0001] The invention relates to the technical field of popping beads for cigarettes, in particular to a method for preparing popping beads for cigarettes from lignin-carbohydrate-coated essence. Background technique [0002] Explosive beads, also known as fragrant pills, brittle capsules, and beads. One or more flavor capsules are pre-installed in the filter tip of pop-pear cigarettes, and the smoker can selectively pinch and pop the capsules to release the flavor during the smoking process. In recent years, domestic tobacco companies have carried out a lot of work in the research and development of popping beads. The core liquid additives in popping beads contain a variety of flavors (fruity, wine, tea, floral, etc.), with different effects. Popping beads are a new way of cigarette flavoring, flavoring and moisturizing technology, which can prevent spices from participating in combustion. Popping beads have a unique closed environment, which can effectively...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): A24B15/30
CPCA24B15/30
Inventor 李栋胡德武黄习文李栓杨娜
Owner HUBEI CHINA TOBACCO IND
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com