Preparation method of waterborne epoxy floor paint
An epoxy floor paint, water-based technology, applied in epoxy resin coatings, chemical instruments and methods, fibrous fillers, etc., can solve the problem of not considering the interface between graphene and water-based epoxy floor paint, poor stability, inability It has been subjected to problems such as acid and alkali erosion for a long time to achieve the effect of prolonging the time of acid and alkali resistance, good performance stability and excellent comprehensive performance.
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preparation example Construction
[0026] A preparation method of water-based epoxy floor paint, characterized in that, comprising the following steps:
[0027] S1. Preparation of modified inorganic filler:
[0028] a. natural cellulose is placed in the reactor, then the temperature in the reactor is raised to 120~140 ℃, the pressure in the reactor is raised to 2~3MPa, and the relative humidity of the air in the control reactor is 88~98 %, after high temperature and high pressure treatment for 2 to 3 minutes, the pressure is quickly released to normal pressure, and the treated natural cellulose is taken out for use;
[0029] b. First, the natural cellulose and graphene powder treated in operation a are immersed in the treatment solution in a ratio of 80 to 90:1 by weight, and the temperature in the treatment solution is kept at 80 to 90 ° C, and the stirring treatment is performed for 30 to 40 minutes. Suction filtration, then put the solid mixture obtained by suction filtration into a cryogenic pulverizer, an...
Embodiment 1
[0044] A preparation method of water-based epoxy floor paint, characterized in that, comprising the following steps:
[0045] S1. Preparation of modified inorganic filler:
[0046] a. The natural cellulose is placed in the reactor, then the temperature in the reactor is raised to 120 ° C, the pressure in the reactor is raised to 2MPa, the relative humidity of the air in the control reactor is 88~98%, high temperature and high pressure After 2 minutes of treatment, the pressure was quickly released to normal pressure, and the treated natural cellulose was taken out for use;
[0047] b. First, the natural cellulose and graphene powder treated in operation a are immersed in the treatment solution according to the weight ratio of 80:1, keep the temperature in the treatment solution at 80°C, stir for 30min, suction filtration, and then pump The filtered solid mixture was put into a cryogenic pulverizer, and pulverized in a liquid nitrogen environment. The speed of the pulverizer w...
Embodiment 2
[0058] A preparation method of water-based epoxy floor paint, characterized in that, comprising the following steps:
[0059] S1. Preparation of modified inorganic filler:
[0060] a. The natural cellulose is placed in the reactor, then the temperature in the reactor is raised to 130 ° C, the pressure in the reactor is raised to 2.5MPa, the relative humidity of the air in the control reactor is 93%, and the high temperature and high pressure treatment After 2.5 minutes, the pressure was quickly released to normal pressure, and the treated natural cellulose was taken out for use;
[0061] b. First, the natural cellulose and graphene powder treated in operation a are immersed in the treatment solution according to the weight ratio of 85:1, keep the temperature in the treatment solution at 85 ° C, stir for 35 minutes, suction filtration, and then pump The filtered solid mixture was put into a cryogenic pulverizer, and pulverized in a liquid nitrogen environment. The speed of the...
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