A kind of plant active ingredient purification method and its application in cosmetics
A technology of active ingredient and purification method, which is applied in the field of cosmetics to achieve the effects of saving cost, enhancing solubility and improving extraction efficiency
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Embodiment 1
[0038] Embodiment 1 A kind of preparation method of Okoume tree resin extract
[0039] Include the following steps:
[0040] S1. Pre-treatment: add 1mol / L NaOH solution to the Okoume resin, adjust the pH value to 8, stir and mix, let stand, separate the liquid, wash the organic phase with water, add a desiccant to dry, and keep it for later use;
[0041] S2. Supercritical fluid extraction: the Okoume tree resin treated in step S1 is extracted by supercritical fluid extraction technology;
[0042] Extraction conditions: extraction pressure: 6MPa; extraction temperature: 32°C; CO 2 Flow rate: 7L / h; extraction time: 1.5h; entrainer: imidazolium-based ionic liquid 1-butyl-3-methylimidazolium hexafluorophosphate, the addition amount is 1wt%;
[0043] S3. Purify the extract: Add 10 mL of the extract obtained in step S2 to 50 mL of ionic liquid (the ionic liquid is 1-propyl-3-methylimidazolium tetrafluoroborate), and pass into the ionic liquid with CO 2 To increase the polarity of...
Embodiment 2
[0046] Embodiment 2 A kind of preparation method of Okoume tree resin extract
[0047] Include the following steps:
[0048] S1. Pretreatment: Add 2mol / L NaOH solution to the Okoume resin, adjust the pH value to 10, stir and mix, let it stand, separate the liquid, wash the organic phase with water, add a desiccant to dry, and retain it;
[0049] S2. Supercritical fluid extraction: the Okoume tree resin treated in step S1 is extracted by supercritical fluid extraction technology;
[0050] Extraction conditions: extraction pressure: 12MPa; extraction temperature: 40°C; CO 2 Flow rate: 12L / h; extraction time: 2.5h; entrainer: imidazolium-based ionic liquid 1-butyl-3-methylimidazolium hexafluorophosphate, the addition amount is 5wt%;
[0051] S3. Purify the extract: Add 10 mL of the extract obtained in step S2 to 50 mL of ionic liquid (the ionic liquid is 1-propyl-3-methylimidazolium tetrafluoroborate), and pass into the ionic liquid with CO 2 To increase the polarity of ionic ...
Embodiment 3
[0053] Embodiment 3 A kind of preparation method of Okoume tree resin extract
[0054] Include the following steps:
[0055] S1. Pretreatment: add 1.5mol / L NaOH solution to the Okoume resin, adjust the pH value to 9, stir and mix, let it stand, separate the liquid, wash the organic phase with water, add a desiccant to dry, and retain it;
[0056] S2. Supercritical fluid extraction: the Okoume resin treated in step S1 is extracted by supercritical fluid extraction technology to obtain an extract;
[0057] Extraction conditions: extraction pressure: 10MPa; extraction temperature: 36°C; CO 2 Flow rate: 10L / h; extraction time: 2h; entrainer is imidazolium-based ionic liquid 1-butyl-3-methylimidazolium hexafluorophosphate, and its addition amount is 3% of the weight of Okoume resin;
[0058] S3. Purify the extract: Add 10 mL of the extract obtained in step S2 to 50 mL of ionic liquid (the ionic liquid is 1-propyl-3-methylimidazolium tetrafluoroborate), and pass into the ionic liq...
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