Liquid laser with adjustable output wavelength, preparation method and application thereof
A liquid and laser technology, which is applied to the parts of liquid lasers, lasers, laser parts, etc., can solve the problems of easy damage, complicated operation, damage, etc., and achieve the effect of great application potential, simple operation and low cost
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[0040] The preparation method of the present invention will be further described in detail in conjunction with specific examples below. It should be understood that the following examples are only for illustrating and explaining the present invention, and should not be construed as limiting the protection scope of the present invention. All technologies realized based on the above contents of the present invention are covered within the scope of protection intended by the present invention.
[0041] The experimental methods used in the following examples are conventional methods unless otherwise specified; the reagents and materials used in the following examples can be obtained from commercial sources unless otherwise specified.
preparation example 1
[0043] Add 10mmol of polyethylene glycol, 1.1mL of water, and 5mmol of ferric chloride into 15mL of ethylene glycol, and stir for 30min to form yellow transparent solution A. Add 12mmol of sodium acetate into 20mL of diethylene glycol and stir for 30min to form a colorless and transparent solution B. Pour solution B into solution A to form solution C, heat and stir, set the temperature at 75°C, and stir for 90 minutes. Finally, the obtained solution was poured into a reaction kettle, put into an oven at 200° C., and reacted for 5 hours. Cool to room temperature, wash several times with ethanol and water to obtain monodisperse ferric oxide nanoparticles, and the scanning electron micrograph is figure 1 .
preparation example 2
[0045] 3 g of polyvinylpyrrolidone was dissolved in 60 mL of water, and then 1 mg of the monodisperse iron ferric oxide nanoparticles prepared in Preparation Example 1 was added into the above solution, and mechanically stirred for 18 hours. The final product was washed several times with ethanol and water to obtain monodisperse ferric oxide nanoparticles coated with polyvinylpyrrolidone, denoted as Fe 3 o 4 @PVP magnetic particles, particle size is 150nm, transmission electron microscope photo is figure 1 illustration in .
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