A method for preparing 3D printed parts with high interplane thermal conductivity

A thermal conductivity, 3D printing technology, applied in 3D object support structures, manufacturing tools, additive manufacturing, etc., can solve problems such as low thermal conductivity, discussion research, filament verification, etc., to achieve improved mechanical properties and good filler dispersion , The effect of reducing the interface thermal resistance

Active Publication Date: 2022-03-01
SICHUAN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the early completion of the paper (2002), no further in-depth discussion and research on the interfacial thermal resistance between the functional filler and the polymer matrix, nor whether it can be used to prepare filaments suitable for FDM 3D printing At the same time, as shown above, the thermal conductivity of the composite material prepared by the final solid phase shear milling is not high only 0.748W / mK, under the same ratio (graphite content is 30wt.% in the PP / YEP35 system), traditional The thermal conductivity of composites prepared by the direct melt blending process is usually about 0.643W / mK, so the thermal conductivity of the former is limited compared to the latter
[0008] Therefore, the existing technology can only be limited to the use of compression molding technology for polymer-based thermally conductive materials that meet industrial standards. The processed products have a simple structure, cannot be continuously produced, and have a long production cycle. It is impossible to give the product a complex porous structure to meet the ventilation of heat conduction; at the same time, due to the constraints of the technology itself during the molding process, defects are easily generated inside the plate product, which affects its performance; mainly, it is fundamentally impossible to obtain high thermal conductivity between the surfaces. Parts, which limit the application range of heat-conducting parts

Method used

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  • A method for preparing 3D printed parts with high interplane thermal conductivity
  • A method for preparing 3D printed parts with high interplane thermal conductivity
  • A method for preparing 3D printed parts with high interplane thermal conductivity

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Effect test

Embodiment 1

[0052] This embodiment adopts a method for preparing a 3D printed part with high thermal conductivity between surfaces, which includes the following steps in parts by weight:

[0053] (1) After mixing 100 parts of low-density polyethylene and 20 parts of graphene nanosheets, add them to a disc-shaped mechanochemical reactor for grinding and pulverization. After the grinding is completed, collect carbon-based fillers and evenly disperse them in the polymer matrix. Composite material powder; among them, the process parameters of the disc-shaped mechanochemical reactor are: the grinding pressure is 30MPa, the temperature of the disc surface is controlled by feeding a constant temperature circulating liquid medium with a temperature of 35°C, cyclic grinding 6 times, and the disc rotation speed 30r / min;

[0054] (2) Extrude the composite material powder obtained in step (1) to obtain a filament for 3D printing. The extrusion processing parameters are: extrusion temperature 170°C, ...

Embodiment 2

[0064] This embodiment adopts a method for preparing a 3D printed part with high thermal conductivity between surfaces, which includes the following steps in parts by weight:

[0065] (1) After mixing 100 parts of low-density polyethylene and 20 parts of carbon nanotubes, they are added to a disc-shaped mechanochemical reactor for grinding and pulverization. After the grinding is completed, carbon-based fillers are collected and evenly dispersed in the polymer matrix. Material powder; among them, the process parameters of the disc-shaped mechanochemical reactor are as follows: the grinding pressure is 25MPa, the temperature of the disc surface is controlled by feeding a constant temperature circulating liquid medium with a temperature of 35°C, and the grinding cycle is 6 times, and the rotational speed of the disc is 30r / min;

[0066] (2) Extrude the composite material powder obtained in step (1) to obtain a filament for 3D printing. The extrusion processing parameters are: e...

Embodiment 3

[0076] This embodiment adopts a method for preparing a 3D printed part with high thermal conductivity between surfaces, which includes the following steps in parts by weight:

[0077] (1) After mixing 100 parts of low-density polyethylene and 40 parts of graphene nanosheets, add them to a disc-shaped mechanochemical reactor for grinding and pulverization. After the grinding is completed, collect carbon-based fillers and evenly disperse them in the polymer matrix. Composite material powder; Among them, the process parameters of the disc-shaped mechanochemical reactor are: the grinding pressure is 30MPa, the temperature of the disc surface is controlled by feeding a constant temperature circulating liquid medium at a temperature of 40°C, and the grinding cycle is 6 times, and the disc rotation speed is 30r / min;

[0078] (2) Extrude the composite material powder obtained in step (1) to obtain a filament for 3D printing. The extrusion processing parameters are: extrusion temperat...

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Abstract

The present invention provides a method for preparing 3D printed parts with high thermal conductivity between surfaces. The preparation method uses the mechanochemical reactor disclosed in the Chinese authorized invention patent ZL 95111258.9 to control pure polymer particles and carbon fillers for heat conduction. Grinding, pulverizing and mixing under the conditions of disc surface temperature, disc pressure and cycle grinding times, then extruding to obtain filaments for 3D printing, and finally preparing 3D printing with high inter-surface thermal conductivity by fused deposition modeling 3D printing parts. The 3D printed product can be prepared by fused deposition modeling 3D printing technology on the basis of high inter-surface thermal conductivity; the preparation method has the characteristics of simple process and continuous production, and is suitable for industrial production of complex structure thermal conductive parts.

Description

technical field [0001] The invention belongs to the technical field of 3D printed parts with interplane thermal conductivity, and specifically relates to a method for preparing 3D printed parts with high interfacial thermal conductivity, especially for the mechanochemical method disclosed in Chinese authorized invention patent ZL 95111258.9. The reactor carries out the preparation of the printing filaments used in the above-mentioned 3D printing parts. Background technique [0002] With the development of modern industry, the microelectronics industry is an important part of it. Electronic devices are becoming increasingly high-speed, integrated, and high-density. They will inevitably generate a lot of heat under working conditions, and electronic devices must be prevented from overheating through heat dissipation. The main purpose of heat dissipation design is to dissipate the heat generated by electronic devices through heat conduction. [0003] General-purpose thermally ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B29C64/118B29C64/314B29B13/10B33Y10/00B33Y40/10
CPCB29C64/118B29C64/314B29B13/10B33Y10/00B33Y40/10
Inventor 陈英红荆晶晶石绍宏熊雨华正坤
Owner SICHUAN UNIV
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