Botanical insecticide for preventing and controlling crop pests and preparation method thereof
A plant-derived insecticide and a technology for crops, which are applied in the field of plant-derived insecticides for preventing and controlling crop pests and the field of preparation thereof, can solve the problems that affect the efficacy of the plant-derived insecticides, the weak emulsification ability of auxiliary agents, and the ineffective persistence. It can achieve high crop systemic and insecticidal activity, not easy to oxidize and volatilize, and good stability.
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Embodiment 1
[0037] A plant-derived insecticide for preventing and controlling crop pests, which is characterized in that it comprises the following components in mass percentage: composite nicotine salt 5%, choline diphosphate / fluorocarbon surfactant 1%, non-ionic surface Active agent 5%, co-solvent 1%, water 88%.
[0038] The preparation method of the compound nicotine salt includes the following steps:
[0039] I. Preparation of organic acid mixture: natural citric acid, natural tartaric acid, glucic acid, natural malic acid and natural quinic acid are mixed uniformly to obtain an organic acid mixture;
[0040] II. Preparation of compound nicotine salt: Put the organic acid mixture obtained in step I into a stirring tank, add propylene glycol and glycerin, mix well, stir and dissolve at 50°C for 20 minutes, then add natural nicotine, stir and react for 4 hours, and cool to At room temperature, compound nicotine salt is obtained.
[0041] In the step I, the molar ratio of natural citric acid, n...
Embodiment 2
[0054] A plant-derived insecticide for preventing and controlling crop pests, which is characterized in that it includes the following components in mass percentages: 8% compound nicotine salt, 1.5% choline diphosphate / fluorocarbon surfactant, non-ionic surface Active agent 6%, co-solvent 2%, water 82.5%.
[0055] The preparation method of the compound nicotine salt includes the following steps:
[0056] I. Preparation of organic acid mixture: natural citric acid, natural tartaric acid, glucic acid, natural malic acid and natural quinic acid are mixed uniformly to obtain an organic acid mixture;
[0057] II. Preparation of compound nicotine salt: Put the organic acid mixture obtained in step I into a stirring tank, add propylene glycol and glycerin, mix well, stir and dissolve at 60°C for 25 minutes, then add natural nicotine, stir and react for 5 hours, and cool to At room temperature, compound nicotine salt is obtained.
[0058] In the step I, the molar ratio of natural citric acid...
Embodiment 3
[0071] A plant-derived insecticide for preventing and controlling crop pests, which is characterized in that it includes the following components in mass percentages: 10% composite nicotine salt, 2% choline diphosphate / fluorocarbon surfactant, and non-ionic surface Active agent 7%, co-solvent 3%, water 78%.
[0072] The preparation method of the compound nicotine salt includes the following steps:
[0073] I. Preparation of organic acid mixture: natural citric acid, natural tartaric acid, glucic acid, natural malic acid and natural quinic acid are mixed uniformly to obtain an organic acid mixture;
[0074] II. Preparation of compound nicotine salt: Put the organic acid mixture obtained in step I into a stirring tank, put in propylene glycol and glycerin, mix well, stir and dissolve at 70°C for 30 minutes, then put in natural nicotine, stir and react for 6 hours, and cool to At room temperature, compound nicotine salt is obtained.
[0075] In the step I, the molar ratio of natural cit...
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