Flexible film-like material for SERS detection and preparation method of flexible film-like material
A technology for detecting flexible and flexible films, which is applied in the fields of analyzing materials, material excitation analysis, and material analysis by optical means. Uniform thickness, easy to wipe sampling effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0029] Embodiment 1 (see figure 1 )
[0030] 1) Preparation of PCL / CS composite solution: Dissolve 0.8g of PCL particles in 9.2g of glacial acetic acid solution at 50°C to obtain 8%wt PCL solution; dissolve 0.2g of CS powder in 9.8g of 90%wt acetic acid at 90°C solution, a 2% wt CS solution was obtained. At 50°C, 3.33g 8%wt PCL was added dropwise to 10g 2%wt CS with a mass ratio of 1:1.5, and stirred at 50°C for 2h to synthesize a PCL / CS solution.
[0031] 2) Preparation of PCL / CS flexible film: inject the PCL / CS solution into the mold, dry it at 50°C to form a film, soak it in 10% NaOH for 5 minutes, rinse and soak it with clean water until the solution is neutral. Finally, dry again in a natural state for later use.
[0032] 3) Preparation of gold seed solution: 0.025mL 0.01M HAuCl 4 solution and 0.6 mL of 0.01M NaBH 4 The solution was added to 1 mL of 0.1M CTAB solution, stirred for 30 min, and left to stand for use.
[0033] 4) Immerse the PCL / CS flexible film cut in...
Embodiment 2
[0037]1) Preparation of PCL / CS composite solution: Dissolve 0.8g of PCL particles in 9.2g of glacial acetic acid solution at 50°C to obtain 8%wt PCL solution; dissolve 0.2g of CS powder in 9.8g of 90%wt acetic acid at 90°C solution, a 2% wt CS solution was obtained. At 50°C, 3.33g 8%wt PCL was added dropwise to 10g 2%wt CS with a mass ratio of 1:1.5, and stirred at 50°C for 2h to synthesize a PCL / CS solution.
[0038] 2) Preparation of PCL / CS flexible film: inject the PCL / CS solution into the mold, dry it at 50°C to form a film, soak it in 10% NaOH for 5 minutes, rinse and soak it with clean water until the solution is neutral. Finally, it was dried again in a natural state for further use, and its morphology was characterized by SEM.
[0039] 3) Preparation of gold seed solution: 0.025mL 0.01M HAuCl 4 solution and 0.6 mL of 0.01M NaBH 4 The solution was added to 1 mL of 0.1M CTAB solution, stirred for 30 min, and left to stand for use.
[0040] 4) Immerse the PCL / CS flexi...
Embodiment 3
[0044] 1) Preparation of PCL / CS composite solution: Dissolve 0.8g of PCL particles in 9.2g of glacial acetic acid solution at 50°C to obtain 8%wt PCL solution; dissolve 0.2g of CS powder in 9.8g of 90%wt acetic acid at 90°C solution, a 2% wt CS solution was obtained. At 50°C, 3.33g 8%wt PCL was added dropwise to 10g 2%wt CS with a mass ratio of 1:1.5, and stirred at 50°C for 2h to synthesize a PCL / CS solution.
[0045] 2) Preparation of PCL / CS flexible film: inject the PCL / CS solution into the mold, dry it at 50°C to form a film, soak it in 10% NaOH for 5 minutes, rinse and soak it with clean water until the solution is neutral. Finally, dry again in a natural state for later use.
[0046] 3) Preparation of gold seed solution: 0.025mL 0.01M HAuCl 4 solution and 0.6 mL of 0.01M NaBH 4 The solution was added to 1 mL of 0.1M CTAB solution, stirred for 30 min, and left to stand for use.
[0047] 4) Immerse the PCL / CS flexible film cut into a suitable size into the gold nanopar...
PUM
Login to view more Abstract
Description
Claims
Application Information
Login to view more - R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap