The invention relates to a method for in-situ preparation of 3D
carbide nanowire arrays by impregnating and
cracking precursors and magnetic pulling method. The three-dimensional
carbide nanowire arrays are synthesized in situ on the surface of
graphite sheets by combining precursor impregnating
cracking and magnetic pulling methods. method. Prepare nano-scale
iron oxide on the surface of high-purity
graphite sheet by co-
precipitation method, and then prepare nano-Fe particles by
hydrogen reduction; then impregnate
graphite sheet containing Fe particles in ZrC precursor, and then heat treatment in a
magnetic field environment. ZrC
nanowire arrays were obtained. The invention has simple preparation method, designable nanowires, no
pollution, safety and stability, improves the field emission performance and
electromagnetic wave absorption performance of the
carbide nanomaterial, reduces the field emission turn-on
voltage of the material, and enhances the combination of the matrix and the
coating. It is widely used in
ceramic matrix composite materials,
resin matrix composite materials, field emitter shoe materials and hard alloys, and has good economic and
social benefits.