Water-based coating composition, coating film, and coated article
A technology of water-based coatings and compositions, applied in the direction of coatings, latex paints, etc., can solve the problems of water resistance reduction and achieve excellent water resistance
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[0131] Hereinafter, although an Example is given and this invention is demonstrated in more detail, this invention is not limited at all by the following Example.
Synthetic example 1
[0133] In a 5-neck flask equipped with a stirrer, reflux condenser, thermometer, dropping device and nitrogen inlet pipe, add 200 parts by mass of ion-exchanged water and 6.0 parts by mass of non-reactive emulsifier a, while purging the reactor with nitrogen For replacement, after raising the temperature to 80°C, 1.0 parts by mass of potassium persulfate was added, and then, 190 parts by mass of methyl methacrylate and 250 parts by mass of butyl acrylate, which had been stirred and mixed in another container in advance, were added dropwise over 3.5 hours. parts, 10 parts by mass of acrylic acid, 220 parts by mass of ion-exchanged water, and 30.0 parts by mass of non-reactive emulsifier a. Then, after aging at 80° C. for 2 hours while continuing to stir, a mixture of 2.7 parts by mass of ion-exchanged water and 0.3 parts by mass of a 70% aqueous solution of tert-butyl hydroperoxide was added to the reactor, and then continuously dripped over 5 minutes. A mixture of 9.7 parts by...
Embodiment 1
[0150] Put 6.5 parts by mass of ion-exchanged water into the mixer, slowly add 1.0 parts by mass of dispersant, 0.2 parts by mass of antifoaming agent, and 20.0 parts by mass of titanium oxide under stirring environment, and mix until the particle size reaches 50 μm or less after the addition is complete. Next, 70.0 parts by mass of the resin dispersion of Synthesis Example 4, 2.0 parts by mass of a viscosity modifier, and 0.3 parts by mass of an antifoaming agent were slowly added to the mixer under stirring environment, and after thorough mixing, the water-based coating composition of Example 1 was obtained.
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