Preparation method of starch apigenin inclusion complex and application of starch apigenin inclusion complex in weight-losing meal replacement food
A technology of meal replacement food and apigenin, which is applied in the application, baked food, baked food with modified ingredients, etc., can solve the problems of long-term consumption, such as unknown hazards, poor absorption, and easy damage by gastric acid. Achieve the effects of improving fat-soluble and water-soluble properties, increasing bioavailability, and low price
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Embodiment 1
[0043]Weigh 20g cornstarch and 4g apigenin respectively, place them in the ceramic tank of planetary ball mill, add auxiliary grinding balls of different sizes according to the mass ratio of balls and mixture close to 2:1, and control the total volume of balls and materials within the total volume of the ball mill tank. Within the range of 1 / 3 to 2 / 3 of the volume, seal the ceramic pot, install it on the ball mill, set the speed at 700r / min, and run the ball mill; after the ball mill has been running for 30 hours, pick out the auxiliary grinding balls, and remove the crude product from the ceramic pot Take it out and weigh 23.45g; wash it twice with absolute ethanol, each time using 234.5mL of ethanol, then filter with suction, dry the filter cake, and weigh 22.83g to obtain the cornstarch apigenin inclusion complex .
[0044] By measuring the content of apigenin in the compound, the content of apigenin in the compound is 71.51 mg / g, and by measuring the digestibility, the dig...
Embodiment 2
[0046] Weigh 20g cornstarch and 4g apigenin respectively, place them in the ceramic tank of planetary ball mill, add auxiliary grinding balls of different sizes according to the mass ratio of balls and mixture close to 2:1, and control the total volume of balls and materials within the total volume of the ball mill tank. Within the range of 1 / 3 to 2 / 3 of the volume, seal the ceramic pot, install it on the ball mill, set the speed at 700r / min, and run the ball mill; after the ball mill has been running for 30 hours, pick out the auxiliary grinding balls, and remove the crude product from the ceramic pot Take out, weighing 23.45g; wash 3 times with absolute ethanol, each ethanol dosage is 234.5mL, then filter with suction, dry the filter cake, weigh 21.49g, and obtain corn starch apigenin inclusion complex .
[0047] By measuring the content of apigenin in the compound, the content of apigenin in the compound is 68.91mg / g, and by measuring the digestibility, the digestibility of...
Embodiment 3
[0049] Weigh 20g cornstarch and 4g apigenin respectively, place them in the ceramic tank of planetary ball mill, add auxiliary grinding balls of different sizes according to the mass ratio of balls and mixture close to 2:1, and control the total volume of balls and materials within the total volume of the ball mill tank. Within the range of 1 / 3 to 2 / 3 of the volume, seal the ceramic pot, install it on the ball mill, set the speed at 800r / min, and run the ball mill; after the ball mill has been running for 35 hours, pick out the auxiliary grinding balls, and remove the crude product from the ceramic pot Take it out and weigh 23.79g; wash it twice with absolute ethanol, each time using 237.9mL of ethanol, then filter with suction, dry the filter cake, and weigh 21.32g to obtain the inclusion complex of cornstarch apigenin .
[0050] By measuring the content of apigenin in the compound, the content of apigenin in the compound is 24.86mg / g, and by measuring the digestibility, the ...
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