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Preparation method of geopolymer pavement repair material resistant to chloride ion erosion

A geopolymer and pavement repair technology, applied in cement production and other directions, can solve problems such as the generation of chloride ions, and achieve the effects of reducing migration and erosion, low requirements for equipment and equipment, and simple and effective methods

Active Publication Date: 2022-07-05
SHANXI KAIDI BUILDING MATERIALS +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The invention overcomes the deficiencies of the prior art, and aims at the problem of using geopolymer repair materials to generate chloride ions, and proposes a preparation method of geopolymer pavement repair materials resistant to chloride ion erosion

Method used

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  • Preparation method of geopolymer pavement repair material resistant to chloride ion erosion

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] The first step will be 400 g Grade fly ash and 20 g of 3-[2-(2-aminoethylamino)ethylamino]propyl-trimethoxysilane were charged into a rubber container, and agate balls were charged as grinding media. The volume ratio of agate balls to sample is 4:1.

[0024] In the second step, the mixed sample mixed with fly ash and 3-[2-(2-aminoethylamino)ethylamino]propyl-trimethoxysilane was placed on a ball mill for ball milling, and the ball mill speed was 400 r / min, continuous rotation for 5h, so that 3-[2-(2-aminoethylamino)ethylamino]propyl-trimethoxysilane is sufficiently and uniformly dispersed on the surface of fly ash to obtain modified fly ash.

[0025] The third step is to weigh 80 g of mineral powder and 20 g of fly ash in a mass ratio of 4:1, weigh 40 g of water glass (modulus 2.2), and 20 g of water, add them to the powder, and stir until the mixture is uniform.

[0026] The fourth step is to pour the above slurry into a mold, and cure it for 56 days at 20 ± 2°C an...

Embodiment 2

[0029] The first step will be 400 g Grade fly ash and 10 g of 3-[2-(2-aminoethylamino)ethylamino]propyl-trimethoxysilane were charged into a rubber container, and agate balls were charged as grinding media. The volume ratio of agate balls to sample is 4:1.

[0030] In the second step, the mixed sample mixed with fly ash and 3-[2-(2-aminoethylamino)ethylamino]propyl-trimethoxysilane was placed on a ball mill for ball milling, and the ball mill speed was 400 r / min, and continuously rotated for 5 h, so that 3-[2-(2-aminoethylamino)ethylamino]propyl-trimethoxysilane was sufficiently and uniformly dispersed on the surface of the fly ash to obtain the modified fly ash.

[0031] The third step is to weigh 80 g of mineral powder and 20 g of fly ash in a mass ratio of 4:1, weigh 40 g of water glass (modulus 2.2), and 20 g of water, add them to the powder, and stir until the mixture is uniform.

[0032] The fourth step is to pour the above slurry into a mold, and cure it for 56 days...

Embodiment 3

[0035] The first step will be 400 g Grade fly ash and 10 g of 3-[2-(2-aminoethylamino)ethylamino]propyl-trimethoxysilane were charged into a rubber container, and agate balls were charged as grinding media. The volume ratio of agate balls to sample is 4:1.

[0036] In the second step, the mixed sample mixed with fly ash and 3-[2-(2-aminoethylamino)ethylamino]propyl-trimethoxysilane was placed on a ball mill for ball milling, and the ball mill speed was 400 r / min, and continuously rotated for 5 h, so that 3-[2-(2-aminoethylamino)ethylamino]propyl-trimethoxysilane was sufficiently and uniformly dispersed on the surface of the fly ash to obtain the modified fly ash.

[0037] The third step is to weigh 80 g of mineral powder and 20 g of fly ash in a mass ratio of 4:1, weigh 40 g of water glass (modulus 2.2), and 20 g of water, add them to the powder, and stir until the mixture is uniform.

[0038] The fourth step is to pour the above slurry into a mold, and cure it for 56 days...

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Abstract

The invention relates to a preparation method of a geopolymer pavement repair material resistant to chloride ion erosion, belonging to the technical field of geopolymers; in particular, it is 3-[2-(2-aminoethylamino)ethylamino]propyl-trimethoxy Silane is uniformly dispersed on the surface of fly ash by ball milling, reacts and is grafted to the surface of fly ash. In the system, it can be attracted by electric charges to prevent the penetration of chloride ions. Fly ash and mineral powder are mixed in a certain proportion. Water glass is added to cause alkali excitation and hydration reaction; the invention has simple synthesis steps, low equipment requirements, simple and effective method, and the prepared geopolymer repair material can effectively prevent the migration and erosion of chloride ions.

Description

technical field [0001] The invention relates to the technical field of geopolymers, in particular to a preparation method of a geopolymer pavement repair material resistant to chloride ion erosion. Background technique [0002] Geopolymer materials have the characteristics of early strength and fast hardening, and can be used as rapid repair materials, such as rapid repair of traffic roads, airport runways, etc., and can also be used for rapid construction of emergency building facilities to improve engineering efficiency. Geopolymer has a unique "cage" structure - a three-dimensional network structure composed of aluminum-oxygen tetrahedron and silicon-oxygen tetrahedron structural units, which can be used for the immobilization of toxic metals and radionuclides, and to solve the leakage of current cement immobilization materials. The problem of high rate and low stability, thereby reducing the possible security risks. Geopolymer materials have excellent corrosion resistan...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B28/00C04B111/20C04B111/72
CPCC04B28/006C04B2111/20C04B2111/72C04B2201/50C04B18/08C04B24/42C04B12/04C04B18/12Y02P40/10
Inventor 王发洲曲敏张平杨锐礼刘鹏杨露胡传林胡曙光
Owner SHANXI KAIDI BUILDING MATERIALS