Preparation method of high-purity feed additive calcium propionate
A feed additive, calcium propionate technology, applied in the field of additive calcium propionate preparation, can solve the problems of CO2 and dust pollution, complicated process, high cost, etc., and achieve the effects of eliminating pollution, simplifying process and protecting the environment
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[0020] A method for preparing a high-purity feed additive calcium propionate, comprising the following steps: (1) Pretreatment: Soak the collected eggshells in lye for 24 hours, rinse them with clean water, and remove the surface of the eggshells. attachments and impurities;
[0021] (2) Shell-membrane separation: add a separating agent to the eggshell, stir, place, pour out the upper solution, and recover it by suction filtration, and then add the recovered filtrate to the precipitate;
[0022] (3) Crush and sieve: Crush the eggshells with a grinder and sieve to make the fineness reach 100 mesh. The unpassed shell materials are crushed again and sieved until all pass through, and bagged for later use;
[0023] (4) Normal temperature and pressure reaction: Weigh an appropriate amount of eggshell powder into a beaker, add tap water, the liquid-solid ratio is 12:1, stir the shell powder solution at a constant speed, and slowly add propionic acid. After the reaction, add calcium ...
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