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A Corrosion Appearance Method of Austenite Grain Size in High Strength Steel

A steel austenite and corrosion display technology, which is applied in the field of corrosion display of high-strength steel austenite grain size, can solve problems such as failure, unclear technical requirements, and inability to correctly grade, etc., to achieve a simple method and clear display Effect

Active Publication Date: 2022-06-24
DONGFENG MOTOR CORP HUBEI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The embodiment of the present invention provides a corrosion display method of austenite grain size in high-strength steel, so as to solve the problem that the display of austenite grain size in the related art is not clear and cannot be correctly rated, resulting in unclear follow-up technical requirements and related failures question

Method used

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  • A Corrosion Appearance Method of Austenite Grain Size in High Strength Steel
  • A Corrosion Appearance Method of Austenite Grain Size in High Strength Steel
  • A Corrosion Appearance Method of Austenite Grain Size in High Strength Steel

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Effect test

Embodiment 1

[0044] (1) Use an electric furnace to smelt the raw materials to ensure that the carbon content in the material at the end of the smelting is less than 0.28%;

[0045] (2) sequentially carrying out ladle refining, vacuum degassing, continuous casting, rolling, and dehydrogenation treatment on the smelted product obtained in step (1) to obtain a billet; wherein, the ladle refining time is greater than 30min; the vacuum degassing time is greater than 20min; the pouring speed of continuous casting is 0.5~0.7m / min; in the rolling process, the material should be heated to above 1150℃, and the rolling speed should be controlled to ensure that the final rolling temperature is greater than 950℃; the temperature of dehydrogenation treatment is 650℃ ; Obtain the blank material (percent by weight) of following chemical composition after dehydrogenation treatment finishes:

[0046] C 0.27%, Si 0.23%, Mn 0.87%, P 0.006%, S 0.003%, Cr 1.52%, Ni 1.46%, Mo 0.24%, Cu 0.07%, Al 0.028%, N 0.013%...

Embodiment 2

[0052] (1) Take the blank obtained in step (2) of Example 1 as a sample, put it into a heating furnace, heat it at a constant temperature of 890±10° C. for 1 hour, take it out and quickly quench it in water.

[0053] (2) The quenched samples are ground and polished in turn.

[0054] (3) Take 80 mL of water to prepare a saturated picric acid solution, and add 3 drops of hydrochloric acid into it to obtain a corrosive agent.

[0055] (4) Put the sample treated in step (2) into a fresh etchant at 85° C. for 9 minutes. During the corrosion process of the entire sample, it is necessary to continuously wipe with a non-woven fabric to prevent corrosion products from accumulating and corroding the metallographic structure in some areas. After the corrosion process was completed, the samples were taken out, rinsed with absolute ethanol and dried.

[0056] (5) Under the metallographic microscope, observe the grain size and grain boundary of the sample, and take pictures and record. Th...

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Abstract

The invention relates to a corrosion display method of high-strength austenite grain size. After the sample is heated at a constant temperature of 890±10°C for at least 1 hour, it is taken out and quickly quenched in water; the quenched sample is sequentially ground and polished; the polished The final sample was corroded in an etchant at 85°C for 9 minutes. During the entire corrosion process, the surface of the sample was continuously wiped with a non-woven cloth; the sample was taken out, rinsed with absolute ethanol and then dried. The invention adds a high-temperature pretreatment step to the sample, then grinds, polishes and corrodes the sample, and finally observes the grain boundary and grain size through a metallographic microscope. The corrosion agent used is prepared from saturated picric acid solution and hydrochloric acid. The metallographic photograph of the sample after the pretreatment step in the present invention shows that the grain boundary is clear and does not show martensitic phase, and the operation is simple.

Description

technical field [0001] The invention relates to the technical field of corrosion, in particular to a corrosion manifestation method of high-strength steel austenite grain size. Background technique [0002] The actual grain size of steel is the austenite grain size obtained under certain heat treatment or hot working conditions, and its actual grain size has a great influence on the mechanical properties and process properties of metal materials. Therefore, it is very important to detect the actual grain size of steel. [0003] Usually, the metallographic etchant of austenitic stainless steel uses nitric acid, hydrochloric acid, and water (water is generally about 70%) according to a certain percentage, or hydrofluoric acid, nitric acid, and water according to a certain volume percentage. The Chinese invention patent application numbered CN101353794A discloses the above-mentioned metallographic etchant. Although this etchant can achieve the purpose of displaying metallograp...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N21/84G01N15/02G01N1/28G01N1/32G01N1/44
CPCG01N21/84G01N15/0205G01N1/286G01N1/32G01N1/44
Inventor 刘傲帆陈然瞿良胡赞付欣怡
Owner DONGFENG MOTOR CORP HUBEI