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Cooling rate controllable titanium alloy wire on-line annealing method and device

A technology of titanium alloy wire and cooling rate, which is applied in the direction of heat treatment process control, furnace type, furnace, etc., can solve the problems of uneven heating, uneven heating, and low efficiency of wire materials, so as to reduce the cooling rate and improve the plasticity of wire materials Effect

Pending Publication Date: 2021-03-26
西安赛特新材料科技股份有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

After decades of exploration, improvement and development, a set of reliable and stable production process of titanium and titanium alloy wire has been formed. At present, there are two typical annealing methods for titanium and titanium alloy wire: one is direct annealing For annealing, that is to coil the wire or bundle the straight wire and put it directly into the pit furnace or vacuum furnace for annealing. Due to the limitation, it is impossible to perform one-time mass annealing. Therefore, to a certain extent, the efficiency is not high; the other is to use online annealing, which is completed by driving the wire into a tube furnace with a certain temperature through a roller group with a certain speed. Annealing solves the problem of uneven heating during direct annealing, and can realize large-scale annealing at one time. However, it is found in production that for small-sized wires, usually with a diameter of Φ≤4mm, the plasticity at room temperature is low, and the performance requirements cannot be met.

Method used

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  • Cooling rate controllable titanium alloy wire on-line annealing method and device

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Set the tubular furnace annealing region 6-1, the buffer 6-2 and the compensation zone 6-3 temperature are 750 ° C, 500 ° C, and 300 ° C, each region is heated, and a thermocouple is provided in each region. Temperature measurement. When the heating is started, when the temperature reaches the set temperature, then after 20 min, the motor 5 is activated, and the set roller is set to 0.38 mm / min, so that the motor 5 is idled for 2min, and the diameter φ is 3.5 mm TC4 disc The wire is passed through the roller 3, and the tube furnace 6 is sent to each heating zone by the tubular furnace, and then exit the tube furnace 6 after the lower section is fed into the tank, finally grind, polished to the finished product. The finished product refers to the GB / T 228.1-2010 to perform a room temperature tensile test and record the elongation, and the tensile test gauge is selected from 100 mm. The results show that after an annealing of the present method and the device, the silk ma...

Embodiment 2

[0032] Set the tube furnace annealing region 6-1, the buffer 6-2 and the compensation area 6-3 temperature are 650 ° C, 450 ° C and 200 ° C, start heating, when the temperature of each zone reaches the set temperature, continues to heat the insulation 20min, start The motor 5 simultaneously sets the roller 3 revolution of 0.38 mm / min to cause the motor 5 to pass through 2min, pass the disk roll TA3 wire of the diameter φ of 3.5 mm through the roller, and feed the tubular furnace 6 to pass the tube. The furnace has a heating zone, and then exit the tubular furnace 6 will be fed into the receiving tank, and finally grind, polished to the finished product. The finished product reference GB / T 228.1-2010 is a room temperature tensile test, and the tensile test gauge is selected to be 100mm. The results show that after an annealing of the online annealing, the wire is increased from 7.0% to 10% compared to the conventional online annealing mode. In the present embodiment, the appara...

Embodiment 3

[0034]The tubular furnace annealing region 6-1 is provided, and the buffer 6-2 and the compensation zone 6-3 are 800 ° C, 500 ° C, and 300 ° C, start heating. When the temperature of each region reaches the set temperature, it continues to heat insulation for 20 minutes. The motor 5 is activated, and the roller 3 rotation speed is set to 0.38 mm / min, so that the motor 5 is idled by 2min, passing the TC4 disc of a diameter φ of 2 mm through the roller 3, and feeds the tube furnace 6 to pass in turn The tube furnace is heated, and then the tube furnace 6 will be sent to the tank, finally grind, and polished to the finished product. The finished product refers to the GB / T228.1-2010 to perform a room temperature tensile test, and the tensile test gauge is selected from 100 mm. The results show that after the online annealing is used to use the method and the device, the silk material elongation is increased from 4.0% to 8% compared to the conventional online annealing mode, and th...

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Abstract

The invention discloses a cooling rate controllable titanium alloy wire on-line annealing method and device. The device is suitable for a titanium alloy wire with the diameter phi of less than or equal to 4 mm, and comprise a tubular furnace, a heating zone of the tubular furnace sequentially comprises an annealing zone, a buffer zone and a compensation zone from front to back, each zone is an independent chamber, all zones communicate through through holes in the axial direction, and the through hole is communicated with the annealing zone; the through holes are used for wires to axially andsequentially penetrate through; a resistance wire is arranged in each zone and used for heating the corresponding zone, and the temperature of the annealing zone is set to be the annealing temperaturevalue of the thin wire; wherein the temperature of the buffer zone is 200-300 DEG C lower than the annealing temperature value; and the temperature of the compensation zone is 200-300 DEG C. According to the device, the cooling rate of the wire after on-line annealing is reduced, so that the plasticity of the small-specification wire is improved, and the use performance of the wire is improved.

Description

[Technical field] [0001] The present invention belongs to the technical field, and more particularly to a controlled method and apparatus for the controlled titanium alloy wire material for cooling rate. 【Background technique】 [0002] Titanium alloys have high specific intensity, good antioxidant, corrosion resistance, and biocompatibility, and their silk products have been widely used in aerospace, weapons, ships and biological implants, and become important rare metals. material. After decades of exploration and development, a set of process has been formed reliable, stable titanium and titanium alloy materials production process. At present, there are two typical titanium and titanium alloy wire annealing methods: one is direct Annealing, that is, the disk wire material or the straight wire material is bundled, directly placed in the ground furnace or vacuum furnace, which is simple, easy to achieve, but the silk is thermally heat, and the body volume is affected by the body ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C21D9/573C21D11/00C22F1/18
CPCC21D9/5732C22F1/183C21D11/005C21D9/0062Y02P10/20
Inventor 杨欢王海魏芬绒罗斌莉杨晓康柳红豆杜晨赵娜英
Owner 西安赛特新材料科技股份有限公司