Electrochromic material and preparation method and application thereof, and battery
An electrochromic material and electrochromic technology, applied in nanotechnology for materials and surface science, chemical instruments and methods, inorganic chemistry, etc.
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[0048] A specific electrochromic material Nb is disclosed in this embodiment 18 W 16 o 93 The preparation method is as follows:
[0049] 1) Dissolve 0.2g of ammonium metatungstate, 0.4914g of niobium oxalate, and 1.0g of citric acid in 2mL of deionized water and 8mL of ethanol, and stir continuously until a homogeneous transparent solution is obtained. While continuing to stir, react at 60°C for 2h A sol-gel precursor solution is obtained.
[0050] 2) Sonicate the FTO conductive glass (20mm*30mm*2.2mm) in acetone, isopropanol, ethanol and deionized water for 10 minutes respectively, purge it with a nitrogen gun, and place it in O 2 Clean in a plasma cleaner for 10 minutes and set aside. The sol-gel precursor solution was uniformly spin-coated on the cleaned FTO conductive glass surface using a spin coater.
[0051] 3) Put the spin-coated thin film attached to the FTO conductive glass in an oven at 150° C. for 1 hour.
[0052] 4) After taking out the film, place it in a m...
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