Active control method for uniform distribution and growth direction of reinforcing phase in particle reinforced titanium-based composite material

A titanium-based composite material and particle reinforcement technology, applied in additive processing, additive manufacturing, etc., can solve the problems of limited precision and size of components, caving and pores, and high defect rate, and achieve improved mechanical properties, wide range of applications, Simple to use effects

Inactive Publication Date: 2021-06-15
INST OF METAL RESEARCH - CHINESE ACAD OF SCI
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, due to the complex forming process of titanium matrix composites, it is difficult to prepare titanium matrix composite components with controllable shape and uniform structure by traditional material preparation technology.
For example: titanium-based composite materials prepared by forging method are difficult to achieve good matching of strong plasticity; titanium-based composite materials prepared by powder metallurgy method have high defect rate in the structure and limited component precision and size; prepared by casting method It is difficult to control the morphology and size of the microstructure and reinforcement phase of titanium matrix composites
At the same time, for components with high reinforcement phase, defects such as cracks, defects, collapse and pores are easily produced during machining, which leads to the scrapping of components

Method used

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  • Active control method for uniform distribution and growth direction of reinforcing phase in particle reinforced titanium-based composite material
  • Active control method for uniform distribution and growth direction of reinforcing phase in particle reinforced titanium-based composite material
  • Active control method for uniform distribution and growth direction of reinforcing phase in particle reinforced titanium-based composite material

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Comparison scheme
Effect test

Embodiment 1

[0032] In this embodiment, the uniform distribution of the reinforcement phase and the active control method of the growth direction in the particle-reinforced TC4-0.05B ​​titanium-based composite material include the following steps:

[0033] (1) Base material preparation: The base material is the substrate used in the laser additive manufacturing process, and its composition is Ti-6Al-4V (wt.%), which is used to prevent the high temperature in the laser additive manufacturing process from causing the formation of the formed component. deformation;

[0034] (2) Forming material preparation: The forming material adopts TC4-0.05B ​​titanium-based composite material pre-alloyed powder, the powder particle size is 15-53 μm, its composition is Ti-6Al-4V-0.05B ​​(wt.%), and the oxygen content is lower than 0.2wt.%;

[0035] (3) Forming process: The forming sample is prepared by laser additive manufacturing. The main process parameters in the forming process are: laser power 130W, ...

Embodiment 2

[0039] In this embodiment, the uniform distribution of the reinforcement phase and the active control method of the growth direction in the particle-reinforced TC4-0.5B titanium-based composite material include the following steps:

[0040] (1) Base material preparation: The base material is the substrate used in the laser additive manufacturing process, and its composition is Ti-6Al-4V (wt.%), which is used to prevent the high temperature in the laser additive manufacturing process from causing the formation of the formed component. deformation;

[0041] (2) Forming material preparation: The forming material adopts TC4-0.5B titanium-based composite material pre-alloyed powder, the powder particle size is 15-53 μm, its composition is Ti-6Al-4V-0.5B (wt.%), and the oxygen content is lower than 0.2wt.%;

[0042] (3) Forming process: The forming sample is prepared by laser additive manufacturing. The main process parameters in the forming process are: laser power 220W, scanning ...

Embodiment 3

[0046] In this embodiment, the uniform distribution of the reinforcement phase and the active control method of the growth direction in the particle-reinforced TC4-1B titanium-based composite material include the following steps:

[0047] (1) Base material preparation: The base material is the substrate used in the laser additive manufacturing process, and its composition is Ti-6Al-4V (wt.%), which is used to prevent the high temperature in the laser additive manufacturing process from causing the formation of the formed component. deformation;

[0048] (2) Forming material preparation: the forming material adopts TC4-1B titanium-based composite material pre-alloyed powder, the powder particle size is 15-53 μm, its composition is Ti-6Al-4V-1B (wt.%), and the oxygen content is lower than 0.2wt .%;

[0049] (3) Forming process: The formed sample is prepared by laser additive manufacturing. The main process parameters in the forming process are: laser power 250W, scanning rate 9...

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Abstract

The invention relates to the field of titanium alloy additive manufacturing, in particular to an active control method for uniform distribution and growth direction of a reinforcing phase in a particle reinforced titanium-based composite material. The method comprises the following steps of 1) preparing a base material; 2) preparing a forming material, wherein the forming material adopts titanium-based composite material pre-alloyed powder, and the oxygen content of the forming material is lower than 0.2%; 3) conducting a forming process, wherein a formed component is prepared in a laser additive manufacturing mode, laser energy density control is adopted in the forming process, and the laser energy density is made to be within the range of 50-350 J / mm<3>; and 4) conducting heat treatment, wherein the formed component is subjected to proper annealing treatment. According to the active control method, active control over distribution and form of the reinforced phase in the particle reinforced titanium-based composite material can be achieved, and the mechanical property of the titanium-based composite material is effectively improved.

Description

technical field [0001] The invention relates to the field of additive manufacturing of titanium alloys, in particular to a method for uniform distribution of reinforcement phases and active control of growth direction in particle-reinforced titanium-based composite materials. Background technique [0002] Ultra-high-speed aircraft technology is the strategic commanding height in the aerospace field in the 21st century, and has become one of the strategic development directions that the world's powerful countries are concerned about. The large-scale exploitation of space plays a vital role and will be widely used in both industrial and military fields. Ultra-high-speed aircraft serve in the atmosphere and complex ionized gas environment, and its sharp nose cone and wing leading edge will experience severe aerodynamic heating process, which will be an extremely severe challenge to the heat-resistant materials and structures of the aircraft, especially for The reliability of c...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F10/28B22F10/36B22F10/64B22F10/85C22C14/00B33Y10/00B33Y40/20B33Y50/02
CPCB22F3/24C22C14/00B33Y10/00B33Y40/20B33Y50/02B22F2003/248
Inventor 蔡雨升吉海宾杨锐任德春雷家峰姜沐池
Owner INST OF METAL RESEARCH - CHINESE ACAD OF SCI
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