Silicone oil modified anti-dazzle anti-reflection coating solution, preparation method and application
An anti-glare and modification technology, applied in the field of solar glass, can solve the problems of not being able to have anti-reflection function at the same time, many processes, etc., and achieve the effects of simple processing, reduction of glare effect, and reduction of production costs.
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preparation example Construction
[0058] The preparation method of the pore-forming agent is as follows: add a certain amount of mixed solvent into a four-necked bottle equipped with a thermometer, an electric stirrer, a condenser tube and a constant pressure funnel, start stirring and heating; when the temperature reaches the preset reaction temperature, , add a certain stoichiometric initiator; after the temperature stabilizes, start adding the pre-weighed mixed monomer, complete the addition of the mixed monomer within the predetermined time, and carry out the heat preservation reaction; after the reaction is completed, cool down to 40 ℃ ~ 50 ℃, add additives to neutralize, adjust the pH value to a suitable range, filter and discharge to obtain a pore-forming agent.
[0059] Specifically, the reaction temperature is 60°C-135°C; the time for adding the mixed monomer is 2-6 hours; the reaction time is 4-16 hours; the pH range of the pore-forming agent is 4-10; the auxiliary agent used for neutralization includ...
Embodiment 1
[0076] Mix 20g of the pore-forming agent of the pore-forming agent synthesis example 1 and 40g of the modified hydroxysilicone oil sol of the synthesis example 3 of the modified hydroxysilicone oil sol, add 0.4g of KH560, stir evenly, heat to 90°C, and keep warm for 2 hour, then cooled to room temperature, added 340g isopropanol, and the solution was diluted to a solid content of 3%, thereby preparing a stable coating solution.
Embodiment 2
[0078] Mix 40g of the pore-forming agent of the pore-forming agent synthesis example 3 with 60g of the modified hydroxysilicone oil sol of the synthesis example 2 of the modified hydroxysilicone oil sol, add 1g of KH550, stir evenly, heat to 50°C, and keep it warm for 8 hours, then After cooling to room temperature, 300 g of isopropanol was added to dilute the solution to a solid content of 4%, thereby preparing a stable coating solution.
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