Medical high-elasticity tin-plated alloy wire and preparation method thereof
A technology of alloy wire and high elasticity, which is applied in the field of high elasticity tin-plated alloy wire for medical use and its preparation, can solve the problems affecting the performance of copper alloy wire, poor elasticity, stress cracks, etc., so as to reduce peeling phenomenon and reduce defects , the effect of increasing strength
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Embodiment 1
[0024] A preparation method of high-elastic tin-plated alloy wire for medical use, first melting the copper base material and alloy particles, adding reinforcing particles, the mass ratio of copper base material, alloy particles, and reinforcing particles is 36:11:0.3, under a pressure of 1.2Mpa Under electromagnetic stirring, and then cast into a copper alloy rod, then wire drawing, annealing, pickling, drying, tinning, to obtain a tinned alloy wire.
[0025] The alloy particles include Pt, and the preparation method is as follows: in 0.5mL concentration of 0.04mol / L containing H 2 PtCl 6 Add 0.032g KI to the DMF solution, stir, add 0.2gPVP and 0.1mL 40wt% methylamine aqueous solution after the solution is clear and bright yellow, heat up to 160°C and react for 13h, cool to obtain a brown-black colloidal solution, separate and dry to obtain velvet Spherical nanoscale Pt particles.
[0026] The reinforcement particles are worm-like carbon fibers; the preparation method of th...
Embodiment 2
[0030] A preparation method of highly elastic tin-plated alloy wire for medical use, first melt copper base material and alloy particles, add reinforcement particles, the mass ratio of copper base material, alloy particles, and reinforcement particles is 56:7:2, under 2Mpa pressure Electromagnetic stirring is carried out, and then cast into a copper alloy rod, followed by wire drawing, annealing treatment, pickling, drying, and tinning to obtain a tinned alloy wire.
[0031] The alloy particles include Pt, and the preparation method is: in 0.5mL concentration of 0.04mol / L H 2 PtCl 6 Add 0.032g KI to the DMF solution, stir, add 0.2g PVP and 0.1mL 40wt% methylamine aqueous solution after the solution is clear and bright yellow, heat up to 150°C and react for 11h, cool to obtain a brown-black colloidal solution, separate and dry to obtain velvet Spherical nanoscale Pt particles.
[0032] The reinforcement particles are worm-like carbon fibers; the preparation method of the rein...
Embodiment 3
[0036] A preparation method of highly elastic tin-plated alloy wire for medical use, first melt the copper base material and alloy particles, add reinforcement particles, the mass ratio of copper base material, alloy particles, and reinforcement particles is 78:14:0.9, under 3Mpa pressure Electromagnetic stirring is carried out, and then cast into a copper alloy rod, followed by wire drawing, annealing treatment, pickling, drying, and tinning to obtain a tinned alloy wire.
[0037] The alloy particles include Pt, and the preparation method is: in 0.5mL concentration of 0.04mol / L H 2 PtCl 6 Add 0.032g KI to the DMF solution, stir, add 0.2gPVP and 0.1mL40wt% methylamine aqueous solution after the solution is clear and bright yellow, heat up to 150-160°C and react for 10-13h, cool to obtain a brown-black colloidal solution, separate, After drying, fluffy nanoscale Pt particles are obtained.
[0038] The reinforcement particles are worm-like carbon fibers; the preparation method...
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