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Instant superfine solid blocky carbon black as well as preparation method and application thereof

An instant-type, carbon black technology, applied in the direction of chemical instruments and methods, fiber types, fibrous fillers, etc., can solve the problems of carbon black dust pollution, dispersion, and endangering the health of operators, and achieve excellent antistatic properties and electrical conductivity properties, solve the agglomeration phenomenon, and the effect of excellent application performance

Active Publication Date: 2021-07-16
SUZHOU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Carbon black has the advantages of low price and wide source of raw materials, but there is serious carbon black dust pollution in the process of production, processing, packaging and transportation of carbon black, which not only deteriorates the production environment, but also seriously affects the health of production workers
In the application process of carbon black powder, there are also problems of carbon black dust pollution and deterioration of the production environment, and according to application requirements, powder carbon black needs to be processed such as emulsification and dispersion, which is extremely inconvenient to use
In order to reduce the environmental pollution of powdered carbon black, carbon black compressors and block carbon black processing devices are used to make block carbon black through mechanical compression (ZL200520033701.1) or extrusion (ZL201820897798.8) to solve the existing Reports on the technical problems that the technology is easy to be scattered in the process of storage and transportation to pollute the environment, and seriously endanger the health of operators in the process of packaging and use
However, in the process of use, there are still deficiencies such as the need to emulsify and disperse powdered carbon black.

Method used

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  • Instant superfine solid blocky carbon black as well as preparation method and application thereof
  • Instant superfine solid blocky carbon black as well as preparation method and application thereof
  • Instant superfine solid blocky carbon black as well as preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0048] 1000 grams of carbon black 15F, 96 grams of dispersant MF, 97 grams of sodium lignosulfonate-N, 34 grams of octadecylamine polyoxyethylene ether (EO=15), 33 grams of Pingpingjia O15 (EO=15), 34 Pre-mix 6 grams of polyether polyol HSH-210, 6 grams of dispersant RQT-FS and 8700 grams of water to prepare a carbon black solution, with a total of 300 grams of additives. The carbon black solution was continuously ground for 2 hours in a zirconia ball mill to obtain a carbon black emulsion. The above-mentioned nano-carbon black emulsion is placed in a container and dried to obtain solid block carbon black.

Embodiment 2

[0050] 1000 grams of carbon black F15, 82 grams of dispersant MF, 81 grams of sodium lignosulfonate-N, 41 grams of octadecylamine polyoxyethylene ether (EO=15), 41 grams of Pingpingjia O15 (EO=15), 41 The carbon black solution was prepared by pre-mixing 1 g polyether polyol HSH-210, 14 g dispersant RQT-FS and 8700 g water. The carbon black solution was continuously ground for 2.5 hours in a zirconia grinding device to obtain a carbon black emulsion. The above-mentioned nano-carbon black emulsion is placed in a container and dried to obtain solid block carbon black.

Embodiment 3

[0052] 2000 grams of carbon black F15, 157 grams of dispersant MF, 157 grams of sodium lignosulfonate-N, 50 grams of octadecylamine polyoxyethylene ether (EO=15), 45 grams of Pingpingjia O15 (EO=15), 78 The carbon black solution was prepared by pre-mixing 1 g of polyether polyol HSH-210, 13 g of dispersant RQT-FS and 7500 g of water. The carbon black solution was continuously ground for 2.5 hours in a zirconia grinding device to obtain a carbon black emulsion. The above-mentioned nano-carbon black emulsion is placed in a container and dried to obtain solid block carbon black.

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Abstract

The invention discloses instant superfine solid blocky carbon black as well as a preparation method and application thereof. The preparation method comprises the steps of pre-mixing powdery carbon black, an anionic surfactant, a nonionic surfactant, a interfacial agent and water, grinding through zirconium oxide, and preparing nano carbon black emulsion with the carbon black particle size not larger than 200 nm; and drying and forming to obtain solid blocky carbon black. The technical scheme provided by the invention has the advantage of no dust pollution, can be conveniently used, and can be quickly dissolved into blocky carbon black which has excellent application performance, is applied to the surface of a material by adopting conventional methods such as padding, coating and the like, and then is dried to prepare a carbon black modified material.

Description

technical field [0001] The invention relates to a preparation technology of a carbon-based material, in particular to the preparation of an environment-friendly solid block carbon black to solve the dust pollution of the existing powdery carbon black. Background technique [0002] Carbon black is an amorphous carbon that is a light, fluffy, very fine black powder with a very high surface area. Carbon black has the advantages of low price and wide source of raw materials, but there is serious carbon black dust pollution in the process of production, processing, packaging and transportation of carbon black, which not only deteriorates the production environment, but also seriously affects the health of production workers. In the application process of carbon black powder, there are also problems of carbon black dust pollution and deterioration of the production environment, and according to application requirements, powdered carbon black needs to be processed such as emulsific...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09C1/56C09C1/58C09C3/08C09C3/10D06M11/74D06M101/32D06M101/38
CPCC09C1/56C09C1/58C09C3/08C09C3/10C09C3/006D06M11/74C01P2004/64C01P2004/62D06M2101/32D06M2101/38
Inventor 石瑜博艾丽候礼文朱亚伟
Owner SUZHOU UNIV
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