White foaming agent with delayed foaming function and preparation method thereof
A foaming agent and functional technology, applied in the field of white foaming agent, can solve the problems of sodium bicarbonate foaming, product performance decline, waste and other problems
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preparation example Construction
[0037] The preparation method of the white blowing agent having delayed foaming function includes the steps of:
[0038] 1) First, the oxidized polyethylene wax emulsion is first manufactured.
[0039] Weighing a certain amount of oxidized polyethylene wax, according to its acid value, calculates the total carboxyl rats therebet, and then prepares the corresponding mass of alkali, water, emulsifier, film forming agent, input according to the total carboxyl rats. In the reactor having a sealing pressurized function, stirring is stirred until the temperature is controlled between 110-200 degrees Celsius, stirred for 15 minutes, then cooling and cooled to prepare an oxidized polyethylene wax emulsion;
[0040] Among them: The number of molar numbers added is larger than the moles containing the carboxyl group contained in the oxidized polyethylene wax; the mass of water is about 110% to 10000% of the oxidized polyethylene wax mass; the emulsifier mass is the quality of oxidized polye...
Embodiment 1
[0068] Example 1 A white foaming agent having delayed foaming function applied to a PVC foam field
[0069] First, the oxidized polyethylene wax (Lianyungang has a new material technology Co., Ltd. 316 # product), 80 grams of potassium hydroxide (Pharmaceutical Group is purified), 3000 g of deionized water, 50 grams of dodecyl benzenesulfonic acid Sodium (Pharmaceutical Group Analysis Pure), 150 grams of flat plus -10 (Jiangsu Hai'an Petrochemical Plant), 100 grams Tween-60 (Wuxi Yatai Joint Chemical Co., Ltd.), 90 grams of oil, spare.
[0070] All materials were added to the reactor having a sealing pressurized heating function, and then stirring the stirring temperature in 2-5 degrees Celsius / min. The speed is controlled between 100-300 rp. When the stirring is continuously stirred to 130 degrees Celsius, the stirring speed is accelerated between 400-700 revolutions. Continue to 130-180 degrees Celsius, preferably between 135-145 degrees Celsius, maintaining the corresponding ...
Embodiment 2
[0072] Embodiment 2 A white foaming agent having delayed foaming function applied to a PS foam field
[0073] Take the oxidized polyethylene wax 1000 grams (Lianyungang has a new material technology Co., Ltd. 719 # product), 80 grams of potassium hydroxide (Pharmaceutical Group is purified), 3000 grams of deionized water, 50 grams of sodium dodecyl benzene sulfonate National Pharmaceutical Group Analysis Pure), 150 grams of flat plus -10 (Jiangsu Hai'an Petrochemical Plant), 100 grams Tween-60 (Wuxi Yatai Joint Chemical Co., Ltd.), 90 grams of oil, spare.
[0074]All materials were added to the reactor having a sealing pressurized heating function, and then stirring the stirring temperature in 2-5 degrees Celsius / min. The speed is controlled between 100-300 rp. When the stirring is continuously stirred to 130 degrees Celsius, the stirring speed is accelerated between 400-700 revolutions. Continue between 140-145 degrees Celsius, maintaining the corresponding temperature and the ...
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