Unlock instant, AI-driven research and patent intelligence for your innovation.

A kind of high density electric fused magnesium oxide and its preparation method and preparation device

A technology for fused magnesia and magnesia, which is applied in the field of its preparation and high-density fused magnesia, can solve the problems of easy cracking, speed up the discharge of impurity components, reduce impurity content, etc., so as to improve corrosion resistance and reduce The effect of smelting unit consumption

Active Publication Date: 2022-05-03
UNIV OF SCI & TECH LIAONING
View PDF6 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] In order to further reduce the unit consumption of smelting, improve the optimized design of the fused magnesia process, and improve the distribution of electrodes on the basis of satisfying the melting requirements; in order to improve the high-temperature corrosion resistance of the existing fused magnesia, it is prone to cracking and surface hardness when used under long-term high temperature The drop phenomenon, by adding zirconium powder and calcium oxide to the magnesia mixture, can form a dense oxide film on the fused magnesia; in order to further improve the quality of magnesia and reduce the impurity content, and further use the AC and DC hybrid melting process to speed up the removal of impurities Component discharge

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A kind of high density electric fused magnesium oxide and its preparation method and preparation device
  • A kind of high density electric fused magnesium oxide and its preparation method and preparation device
  • A kind of high density electric fused magnesium oxide and its preparation method and preparation device

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0041] A method for preparing high-density electric fused magnesium oxide, the specific process steps are as follows:

[0042] Step 1, crushing the magnesite ore to less than 80 mm to obtain magnesium oxide raw material;

[0043] Step 2, adding 0.01-0.5wt% zirconium powder and 0.01-0.05wt% calcium oxide to the magnesium oxide raw material, the particle size of the zirconium powder is 0.1-100 μm, and mixing uniformly to obtain product 1;

[0044] Step 3, crushing the carbon block electrode to less than 50 mm to obtain the electrode raw material;

[0045] Step 4, in terms of mass percentage, spread 10-15wt% of the product one on the bottom of the electric furnace, and spread 10-15wt% of the electrode raw material on the area around the cylindrical electrode at the bottom of the center of the electric furnace; The three live wire electrodes of the electric melting furnace are randomly named as the first electrode, the second electrode and the third electrode. 100; the cross-sec...

Embodiment 1

[0059] On the basis of the disclosed embodiments, a method for preparing high-density electric fused magnesia is disclosed. The magnesite ore with a magnesite content of 46.7% is crushed in a jaw crusher to a size below 80 mm, and the magnesia raw material is added to account for The total mass is 0.01wt% zirconium powder and 0.01wt% calcium oxide, and the particle size of the zirconium powder is 0.1-10 μm; the carbon block electrode is crushed in a jaw crusher to less than 50 mm to obtain a carbon block electrode; in mass percentage, the 10wt% of the product is spread on the bottom of the electric melting furnace, and then 10wt% of the electrode raw material is spread in the area around the cylindrical electrode at the bottom of the center of the electric melting furnace. Add evenly near the solid graphite electrode at a melting temperature of 2000°C, and continue to melt for 1 hour; add 50wt% magnesium oxide raw materials evenly near the solid graphite electrode at a melting ...

Embodiment 2

[0071] On the basis of the disclosed embodiments, a method for preparing high-density electric fused magnesia is disclosed. The magnesite ore with a magnesia content of 48% is crushed in a jaw crusher to a size below 80mm, and the magnesia raw material is added to account for The total mass is 0.5wt% zirconium powder, and 0.05wt% calcium oxide, and the particle size of the zirconium powder is 60-100 μm; the carbon block electrode is crushed to below 50 mm in a jaw crusher to obtain a carbon block electrode; in mass percentage, the 15wt% of the product is spread on the bottom of the electric melting furnace, and then 15wt% of the electrode raw material is spread in the area around the cylindrical electrode at the bottom of the center of the electric melting furnace. Evenly added to the vicinity of the solid graphite electrode at a melting temperature of 2000°C, and continued for 12 hours; DC power supply evenly added 30wt% magnesium oxide raw materials to the vicinity of the sol...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
particle sizeaaaaaaaaaa
particle diameteraaaaaaaaaa
particle diameteraaaaaaaaaa
Login to View More

Abstract

The invention relates to the technical field of inorganic chemical industry, in particular to a high-density fused magnesia, a preparation method and a preparation device thereof. The invention relates to a high-density electric fused magnesium oxide and a preparation method thereof. The preparation method comprises: crushing, mixing, alternating current electric melting, direct current electric melting and natural cooling to prepare the following finished products. The product and process of the present invention have the following characteristics: the distribution law of the electrodes is improved to further reduce the unit consumption of smelting; the addition of zirconium powder and calcium oxide to the magnesia mixture can form a dense oxide film in the fused magnesia, which improves Corrosion resistance; the hollow electrode design helps the impurity components to be discharged from the inside; the two-stage electrofusion process of alternating current and then direct current helps to ensure that the impurities and magnesium oxide are separated for a long time, and the alternating current helps the impurities to be kept in an uninterrupted state. The stable state is easily discharged from the hollow electrode, which improves the quality of magnesium oxide and further expands the application range, which has obvious practical value.

Description

technical field [0001] The invention relates to the technical field of inorganic chemical industry, in particular to a high-density fused magnesia, a preparation method and a device thereof. Background technique [0002] The fused magnesium material has a high melting point (2800°C), large crystal grains, compact structure, strong slag resistance, high temperature resistance, stable chemical properties, high compressive strength, strong insulation performance, erosion resistance, and corrosion resistance. The crystal is about 2300 It is widely used in high-temperature electrical insulation materials, and is also an important raw material for making high-grade magnesia bricks, magnesia-carbon bricks and amorphous refractory materials. Based on the excellent characteristics of fused magnesia, it is widely used It is used in high-temperature electrical insulation materials, and is also an important raw material for making high-grade magnesia bricks, magnesia-carbon bricks and u...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C04B2/10
CPCC04B2/102C04B2/104
Inventor 李振郭丽莉王晓民高爽陈晓陆李世强邵思佳朱晓航张全庆陈娜赵致如唐开钰王一董豪曲佳林
Owner UNIV OF SCI & TECH LIAONING