Acrylate pressure-sensitive adhesive, oriented polystyrene expansion adhesive tape as well as preparation method and application thereof
A technology of acrylate and dimethacrylate, which is used in oriented polystyrene expanded tape and its preparation, and in the field of acrylate pressure-sensitive adhesive, can solve the problem of unstable viscosity, inability to meet the use environment of electrolyte resistance, and unfavorable stable operation of batteries And other issues
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preparation example Construction
[0026] The preparation monomer of the above-mentioned acrylate pressure sensitive adhesive includes a specific content of acrylate soft monomer, acrylate hard monomer, crosslinking monomer and functional monomer, and the functional monomer is selected from 3 (ethoxy) bisphenol A At least one of dimethacrylate, 2 (ethoxy) bisphenol A dimethacrylate, and 4 (ethoxy) bisphenol A dimethacrylate. By introducing 0.1wt% to 3wt% of the prepared monomer into the pressure-sensitive adhesive, a specific type of functional monomer containing bisphenol A group has good compatibility with acrylate prepolymers, and by polymerizing The reaction types bisphenol A functional groups into the polymer backbone of acrylate pressure-sensitive adhesives, giving acrylate pressure-sensitive adhesives excellent chemical resistance, corrosion resistance, heat resistance and weather resistance, and controlling glass transition temperature At -40℃~-30℃, the chemical resistance, corrosion resistance, heat re...
Embodiment 1
[0064] 1. To prepare the pressure-sensitive adhesive for oriented polystyrene expansion tape, the glass transition temperature of the formula in this example is Tg=-33.3°C, and each component is weighed according to the formula shown in Table 1:
[0065] The acrylate pressure sensitive adhesive component formula of table 1 embodiment 1
[0066]
[0067]
[0068] The acrylate pressure-sensitive adhesive of the present embodiment is prepared according to the following steps:
[0069] 1) respectively take by weighing each component according to the formula of table 1;
[0070] 2) nitrogen is passed into the reaction kettle to discharge air, then 80% of the solvent is added to the reaction kettle, and the temperature is raised to 78 ℃~80 ℃ reflux;
[0071] 3) adding the prepared monomer into the feeding kettle, then dissolving 80% of the initiator with 10% of the solvent and adding it to the feeding kettle, stirring evenly, to obtain the mixed prepolymerized monomer;
[00...
Embodiment 2
[0080] 1. To prepare the pressure-sensitive adhesive for oriented polystyrene expansion tape, the glass transition temperature of the formula in this example is Tg=-36.3°C, and each component is weighed according to the formula shown in Table 2:
[0081] The acrylate pressure sensitive adhesive component formula of table 2 embodiment 2
[0082]
[0083] The acrylate pressure-sensitive adhesive of the present embodiment is prepared according to the following steps:
[0084] 1) respectively take each component according to the formula of table 2;
[0085] 2) nitrogen is passed into the reaction kettle to discharge air, then 80% of the solvent is added to the reaction kettle, and the temperature is raised to 78 ℃~80 ℃ reflux;
[0086] 3) adding the prepared monomer into the feeding kettle, then dissolving 80% of the initiator with 10% of the solvent and adding it to the feeding kettle, stirring evenly, to obtain the mixed prepolymerized monomer;
[0087] 4) adding 20% of t...
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