Humidity-adjustable hydrogel colorful structural color preparation method
A hydrogel and structural color technology, applied in the field of nano-structural color, can solve the problems of complicated operation and difficult regulation, and achieve the effect of low exposure pressure and low exposure
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Embodiment 1
[0030] A method for preparing a hydrogel colorful structural color with adjustable humidity, comprising the following steps:
[0031] a) Depositing a 100nm-thick underlying metal aluminum layer on a clean silicon substrate by thermal evaporation;
[0032] b) Disperse polyvinyl alcohol with a molecular weight of 20,000 g / mol in deionized water, heat and stir until dissolved, and configure a solution with a concentration of 10%;
[0033] c) Utilize the uniform coating technology, evenly spin-coat a 10% polyvinyl alcohol solution on the metal aluminum layer of the silicon substrate, and form a middle layer of polyvinyl alcohol hydrogel with a thickness of 300nm by controlling the uniform speed of 3000 rpm Floor;
[0034] d) Using electron beam exposure technology, the operating conditions are: exposure high voltage 5kv, grating size 30μm, 1000μC / cm on the hydrogel film 2 Electron beam exposure; electron beam irradiation causes the cross-linking of hydrogel molecules, resulting ...
Embodiment 2
[0038] The difference from Example 1 is that the thickness of the polyvinyl alcohol hydrogel layer of the middle layer in step c) is 133nm.
Embodiment 3
[0040] The difference from Example 1 is that the thickness of the polyvinyl alcohol hydrogel layer of the middle layer in step c) is 184nm.
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Abstract
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