Method for preparing anti-wrinkle real silk fabric

A technology for silk fabrics and wrinkled silk is applied in the field of preparation of functional textiles, which can solve the problems affecting the consumption of silk fabrics, low elasticity of silk fibers, low elastic recovery rate, etc. /S value increase effect

Pending Publication Date: 2021-11-02
JIANGSU HUAJIA SILK +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Silk fabrics are favored by consumers because of their elegant luster, light and elegant style, soft feel and excellent wearing comfort. However, due to the low elasticity of silk fibers, especially the low elastic recovery rate, ord

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Method for preparing anti-wrinkle real silk fabric

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Step 1: Silk fabric pretreatment, experimental plan: silk fabric 10cm×10cm, 60°C, soap flakes 2g / L, NaHCO 3 5g / L, liquor ratio 1:50, boiled in water for 30min, and dried in vacuum at 60°C. Then use acetone, ethanol, and deionized water to wash with ultrasonic vibration, and ultrasonically wash each solution for 20 minutes. After washing, take out the cloth sample and dry it in vacuum at 60°C.

[0026] Step 2: Preparation of pyrimidine derivative dispersion emulsion method, experimental scheme: Add Span 20 (20% o.w.t) and Tween 80 (30% o.w.t) into 100 mL of water, and emulsify at a speed of 10000 rpm for 30 min. During this process, 10% (o.w.f) 2,4,6-trichloropyrimidine compound was slowly added to the solution. Water was then added to dilute the emulsion to obtain a 3 g / L solution. Finally, silicone defoamer, 2 g / L sodium sulfate (catalyst) and 6 g / L sodium bicarbonate were added to each diluent and stirred uniformly to prepare a uniform dispersion of the pyrimidine c...

Embodiment 2

[0029] Step 1: Silk fabric pretreatment, experimental plan: silk fabric 10cm×10cm, 60°C, soap flakes 2g / L, NaHCO 3 5g / L, liquor ratio 1:50, boiled in water for 30min, and dried in vacuum at 60°C. Then use acetone, ethanol, and deionized water to wash with ultrasonic vibration, and ultrasonically wash each solution for 20 minutes. After washing, take out the cloth sample and dry it in vacuum at 60°C.

[0030] Step 2: Preparation of pyrimidine derivative dispersion emulsion method, experimental scheme: Add Span 20 (20% o.w.t) and Tween 80 (30% o.w.t) into 100 mL of water, and emulsify at a speed of 10000 rpm for 30 min. During this process, 10% (o.w.f) 2,4,6-trichloropyrimidine compound was slowly added to the solution. Water was then added to dilute the emulsion to obtain a 3 g / L solution. Finally, silicone defoamer, 2 g / L sodium sulfate (catalyst) and 6 g / L sodium bicarbonate were added to each diluent and stirred uniformly to prepare a uniform dispersion of the pyrimidine c...

Embodiment 3

[0033] Step 1: Silk fabric pretreatment, experimental plan: silk fabric 10cm×10cm, 60°C, soap flakes 2g / L, NaHCO 3 5g / L, liquor ratio 1:50, boiled in water for 30min, and dried in vacuum at 60°C. Then use acetone, ethanol, and deionized water to wash with ultrasonic vibration, and ultrasonically wash each solution for 20 minutes. After washing, take out the cloth sample and dry it in vacuum at 60°C.

[0034] Step 2: Preparation of pyrimidine derivative dispersion emulsion method, experimental scheme: add Span 20 (20% o.w.t) and Tween 80 (30% o.w.t) into 100-150 mL of water, and emulsify at a speed of 10000 rpm for 30 minutes. During this process, 10% (o.w.f) 2,4,6-trichloropyrimidine was slowly added to the solution. Water was then added to dilute the emulsion to obtain a 3 g / L solution. Finally, silicone defoamer, 2 g / L sodium sulfate (catalyst) and 6 g / L sodium bicarbonate were added to each diluent and stirred uniformly to prepare a uniform dispersion of the pyrimidine co...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention provides a method for preparing an anti-wrinkle real silk fabric, and belongs to the field of surface grafting modification of textiles. The method specifically comprises the steps that firstly, the real silk fabric is pretreated, pyrimidine derivatives are adopted to modify the real silk fabric, the pyrimidine derivatives are grafted to the real silk fabric, and the wet-state wrinkle resistance of the real silk fabric is improved; and in addition, the K/S value of the real silk fabric obtained after dyeing modification of the reactive dye is improved, it is indicated that the modified real silk fabric has good dyeing performance, and the dyeability of the cotton fabric can be improved.

Description

technical field [0001] The invention belongs to the technical field of preparation methods of functional textiles, and in particular relates to a method for preparing anti-wrinkle silk fabrics. Background technique [0002] Silk fabric generally refers to silk, including mulberry silk, tussah silk, castor silk, tapioca silk, etc. Silk fabrics are favored by consumers because of their elegant luster, light and elegant style, soft feel and excellent wearing comfort. However, due to the low elasticity of silk fibers, especially the low elastic recovery rate, ordinary silk fabrics are used The fabric made is more prone to wrinkling and difficult to restore to its original shape after wrinkling, and its wrinkle resistance is poor, which affects the consumption of real silk fabrics to a large extent. Improving the wrinkle resistance of silk fabrics is an important direction to increase its added value. [0003] There are two ways to improve the wrinkle resistance of fabrics. One...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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IPC IPC(8): D06M13/355D06M101/12
CPCD06M13/355D06M2200/20D06M2101/12
Inventor 陈国强李敏华董雪楚润善李刚邢铁玲关晋平俞金键
Owner JIANGSU HUAJIA SILK
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