Thermosetting lens composition, thermosetting lens, and manufacturing method thereof
A thermal curing and composition technology, applied in glasses/goggles, instruments, optics, etc., can solve problems such as process safety doubts, poor wear resistance and impact resistance, and easy explosion
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[0095] The preparation method of the heat-curable lens composition as described herein is to use a heat-curing program to cure for about 20-24 hours, including the following steps:
[0096] S1. The heat-curable lens composition is mixed into a glue solution according to the ratio as claimed in claim 2, and vacuum defoaming is performed to form a first mixture;
[0097] S2. injecting the first mixture into a light-transmitting mold to form a mold body, and heating the mold body to form a second mixture;
[0098] S3. performing temperature-controlled curing on the second mixture to form a heat-cured lens;
[0099] S4. Release and dry the heat-cured lens in S3, and perform secondary curing to obtain the heat-cured lens.
[0100] In another preferred example, the vacuum defoaming in S1 lasts for 30 minutes at room temperature and a pressure less than 0.1 torr.
[0101] In another preference, a demoulding step can be added after forming the second mixture;
[0102] In another pr...
Embodiment 1
[0109] Example 1. Preparation of thermosetting lenses
[0110] Example 1 is prepared according to the list of reagents in Table 1 and Table 2. After the reagents are mixed evenly with the listed weight parts, the obtained glue is prepared according to the following steps to prepare thermosetting lenses:
[0111] (1) Put the thermosetting lens composition into a vacuum oven at room temperature and defoam in vacuum for 30 minutes at a pressure of less than 0.1 torr to form a first mixture).
[0112] (2) injecting the first mixture into a light-transmitting mold to form a mold body, and heating the mold body to form a second mixture. The heating program used was:
[0113] First raise the temperature of the mold body from room temperature to 41°C, and heat it at 41°C for 11 hours; then raise the temperature of the mold body from 41°C to 110°C, and heat it at 110°C for 8 hours; ℃ to 55 ℃, and continue for 1 hour
[0114] (3) Perform temperature-controlled curing on the second mi...
Embodiment 2 to 5
[0117] Examples 2 to 5: Preparation of thermosetting lenses
[0118] Examples 2 to 5 are based on the reagents and dosages listed in Table 1, using the same method as in Example 1 to mix evenly and carry out glue injection molding to form a mold body, and then release the mold after curing, and perform the following lenses The evaluation items, and the results are shown in Table 3.
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