Electrolyte membrane for all-solid-state battery, and all-solid-state battery including same
A technology of all-solid-state batteries and solid electrolyte membranes, applied in the direction of non-aqueous electrolyte batteries, non-aqueous electrolyte battery electrodes, solid electrolytes, etc., can solve problems such as short circuits, and achieve the effects of improved life characteristics and uniform ion conductivity
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Embodiment 1
[0085] (1) Prepare the lower solid electrolyte membrane layer
[0086] Polyethylene oxide (PEO) (Mw=4,000,000 g / mol) was dissolved in a solvent of acetonitrile (AN) to prepare a 4% by weight polymer solution. In this case, the addition of lithium salt LiTFSI makes [EO] / [Li + ]=18 / 1 (molar ratio). The polymer solution was stirred overnight at 70 °C to fully dissolve the PEO and lithium salt. Subsequently, an additive solution including an initiator and a curing agent is prepared. The curing agent is polyethylene glycol diacrylate (PEGDA) (Mw=575), and the initiator is benzoyl peroxide (BPO). PEGDA was present in an amount of 20% by weight based on PEO and BPO was present in an amount of 1% by weight based on PEGDA. The solvent used was acetonitrile. The additive solution was stirred for about 1 hour to thoroughly mix the added ingredients. Subsequently, the additive solution was added to the polymer solution and the two solutions were thoroughly mixed together. Spread an...
Embodiment 2
[0094] A solid electrolyte membrane was prepared in the same manner as in Example 1, except that, in the preparation of the solid electrolyte membrane, the concentration of the guiding material was 2% by weight.
Embodiment 3
[0096] A solid electrolyte membrane was prepared in the same manner as in Example 1, except that, in the preparation of the solid electrolyte membrane, polystyrene-block-poly(2-vinylpyridine) (S2VP, PS Mn 133kg / mol , P2VP Mn 132kg / mol) as a block copolymer for the guiding layer.
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