Efficient reduction repairing agent for asphalt pavement, preparation method and application
A technology of asphalt pavement and repair agent, applied in the direction of asphalt coating and coating, which can solve the problems of loose aggregate on the surface of the pavement, slow driving speed and large water seepage coefficient.
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Embodiment 1
[0021] Example 1 Asphalt Pavement Efficient Restoration Agent
[0022] S1. Preparation of acrylic acid polymer grafted with 2-(1-cyclopentenyl) acetic acid side chains: Add 50 parts of ethylene glycol dimethyl ether into the reactor, heat up to 110°C under nitrogen flow, then stir and drop Comprising 52 parts of polypropylene glycol (meth)acrylate, 6.5 parts of polyethylene glycol mono(meth)acrylate and 1 part of tert-butyl peroxy-2-ethylhexanoate, after the dropwise addition, the React at 110°C for 0.5-3h to obtain an acrylic acid polymer with a Mw of 8000, add 0.6 parts of 2-(1-cyclopentenyl)acetic acid dropwise to the acrylic polymer, and react at 40-50°C for 0.5-2h to obtain 2- (1-cyclopentenyl) acetic acid side chain grafted acrylic acid polymer;
[0023] S2. Preparation of polymer emulsion: Dissolve 8-15 parts of methacryloyloxyethyltrimethylammonium chloride and 0.1-2 parts of benzenesulfonic acid in water, and add 5-12 parts of tetramethylammonium under stirring condi...
Embodiment 2
[0026] Example 2 Asphalt Pavement Efficient Restoration Agent
[0027] S1. Preparation of acrylic acid polymer grafted with 2-(1-cyclopentenyl) acetic acid side chains: Add 50 parts of ethylene glycol dimethyl ether into the reactor, heat up to 110°C under nitrogen flow, then stir and drop Comprising 52 parts of polypropylene glycol (meth)acrylate, 6.5 parts of polyethylene glycol mono(meth)acrylate and 1 part of tert-butyl peroxy-2-ethylhexanoate, after the dropwise addition, the React at 110°C for 0.5-3h to obtain an acrylic acid polymer with a Mw of 8000, add 0.6 parts of 2-(1-cyclopentenyl)acetic acid dropwise to the acrylic polymer, and react at 40-50°C for 0.5-2h to obtain 2- (1-cyclopentenyl) acetic acid side chain grafted acrylic acid polymer;
[0028] S2. Preparation of polymer emulsion: Dissolve 15 parts of sodium vinylsulfonate and 2 parts of sulfuric acid in water, add 12 parts of vinyltrimethoxysilane and 35 parts of 2-(1-cyclopentenyl) under stirring condition ...
Embodiment 3
[0031] Example 3 Asphalt Pavement Efficient Restoration Agent
[0032] S1. Preparation of acrylic acid polymer grafted with 2-(1-cyclopentenyl) acetic acid side chains: Add 50 parts of ethylene glycol dimethyl ether into the reactor, heat up to 110°C under nitrogen flow, then stir and drop Comprising 52 parts of polypropylene glycol (meth)acrylate, 6.5 parts of polyethylene glycol mono(meth)acrylate and 1 part of tert-butyl peroxy-2-ethylhexanoate, after the dropwise addition, the React at 110°C for 0.5-3h to obtain an acrylic acid polymer with a Mw of 8000, add 0.6 parts of 2-(1-cyclopentenyl)acetic acid dropwise to the acrylic polymer, and react at 40-50°C for 0.5-2h to obtain 2- (1-cyclopentenyl) acetic acid side chain grafted acrylic acid polymer;
[0033] S2. Preparation of polymer emulsion: 12 parts of methacryloyloxyethyltrimethylammonium chloride and 0.5 part of benzenesulfonic acid are dissolved in water, and 8 parts of phenyltrimethoxysilane and 32 parts of phenyltr...
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