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Multifunctional paste and preparation method thereof

A multi-functional and functional technology, applied in the direction of magnetic/electric field shielding, electrical components, etc., can solve the problems of mechanical performance decline, stirring difficulty, system viscosity increase, etc., and achieve long-lasting and stable antistatic performance, strong practicability, and good mechanical performance Effect

Active Publication Date: 2022-01-04
JIANGXI COPPER TECHNOLOGY RESEARCH INSTITUTE CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the solution proposed by the author to add an appropriate dispersant has the following disadvantages: (1) the antistatic agent with a huge specific surface area can have an oil absorption value several times that of its own weight, and cause the viscosity of the system to increase significantly and make it difficult to stir. Lead to uneven distribution of antistatic agent in multifunctional paste products, antistatic instability and other defects
(2) The addition of a dispersant can indeed reduce the viscosity of the multifunctional paste dipping solution. However, if you want to obtain a uniform multifunctional paste dipping solution under relatively simple conditions (such as simple mechanical stirring), you must add a large amount of dispersant for Due to the dispersion of the antistatic agent, this will inevitably lead to the softening of the multifunctional paste product and the decline in mechanical properties

Method used

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  • Multifunctional paste and preparation method thereof
  • Multifunctional paste and preparation method thereof
  • Multifunctional paste and preparation method thereof

Examples

Experimental program
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Effect test

preparation example Construction

[0051] S1) Preparation of plasticizer emulsion;

[0052] S2) Carbon nanotube shear dispersion, dispersion concentration and drying;

[0053] S3) Preparation of multi-functional paste.

[0054] The specific steps of S1) are:

[0055] S1.1) In accordance with the design component, each material is weighed, and the environmentally friendly plasticizer is mixed with the emulsifier after the rotational speed is 500 ~ 3000R / min, the emulsification time is from 1 to 30 minutes.

[0056] After S1.2), the addition of anhydrous ethanol of the environmentally friendly plasticized dose is added, and the high-speed shear emulsification of the emulsified pump is activated 1 to 30 min, i.e., obtain a plasticizer emulsion.

[0057] The specific steps of S2) are:

[0058] S2.1) In the middle plasticizer emulsion obtained by adding carbon nanotubes to S1.2, at a rotational speed of 500 to 2000 r / min, the shear is dispersed from 1 to 30 minutes to obtain a dispersion;

[0059] S2.2) The dispersi...

Embodiment 1

[0065] 50 DOTP plasticizers were mixed with 0.1 parts of polyether silicone emulsifier, slightly stirred, and transferred to an emulsified pump for strong emulsification for 3 min. After the mixing was completed, it was poured into a 5L container having 200 parts of ethanol to form a coarse dispersion emulsion. The high-speed dispersing machine is opened, maintaining the rotational speed at 1500r / min, using high-speed mixing pad to cut the coarsely dispersed emulsion to disperse 10 min to obtain a micro-nanotic emulsion. After reaching the predetermined mixing time, stop stirring, add 10 multi-walled carbon nanotubes to the emulsion GT300, continued to stir at high speed to disperse 20 min, stop stirring again. The transfer of free ethanol was separated from the mixed liquid transfer after the secondary dispersion to obtain a concentrated paste. The concentrated paste was transferred to an oven at 110 ° C, baked for 8 h. After collecting the fully dried material, transfer to th...

Embodiment 2

[0067] 100 parts of DINCH plasticizer were mixed with 1 part of alkylphenol polyoxyethylene ether emulsifier, and after stirring, transferred to an emulsion pump for strong emulsion mixing for 3 min. After the mixing was completed, it was poured into a 5L container having 1000 parts of ethanol to form a coarse dispersion emulsion. The high-speed dispersing machine is opened, maintaining the rotational speed at 1500r / min, using high-speed mixing pad to cut the coarsely dispersed emulsion to disperse 10 min to obtain a micro-nanotic emulsion. After the predetermined agitation time is reached, stir it, and 50 parts of multi-walled carbon nanotubes are added to the emulsion. NC7000, continued to stir the dispersion of 20 min after high speed, stop stirring again. The transfer of free ethanol was separated from the mixed liquid transfer after the secondary dispersion to obtain a concentrated paste. The concentrated paste was transferred to an oven at 110 ° C, baked for 8 h. After co...

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Abstract

The invention belongs to the technical field of materials, and particularly relates to multifunctional paste and a preparation method thereof. The multifunctional paste comprises the following components in percentage by mass: 50-70% of PVC paste resin powder, 20-40% of a paste resin plasticizer and 0.1-10% of a high-dispersion carbon nanotube composition. The preparation method comprises the steps of preparing a plasticizer emulsion; shearing and dispersing the carbon nanotubes; concentrating and drying the dispersion; and preparing the multifunctional paste. The multifunctional paste has the beneficial effects that the high-dispersion carbon nanotube composition used in the preparation process of the multifunctional paste forms a high-dispersion carbon nanotube-emulsion dispersion under the promotion of high-speed shearing and interaction force between micro-nano emulsion-carbon nanotube bundles and environment-friendly plasticizer molecules. The high-dispersion carbon nanotube composition does not pulverize, does not leak oil, is high in dispersion, is convenient to use, and is especially suitable for the fields of low-toxicity, healthy, environment-friendly and safe permanent antistatic, conductive and electromagnetic shielding.

Description

Technical field [0001] The present invention belongs to the field of material technology, and more particularly to a multi-functional paste and a preparation method thereof. Background technique [0002] At present, the polyvinyl chloride (PVC) paste resin powder is mixed with a plasticizer and form a stable suspension after stirring, referred to as PVC plastic paste. The PVC plastic paste is only relying on heating to a PVC product. The PVC plasticized paste material is convenient, stable performance, excellent product performance, good chemical stability, has a certain mechanical strength, easy color, widely used in gloves, wallpapers, curtains, artificial leather, silicone toys, soft trademarks, Wallpaper, paint coatings, foaming plastic and other fields. [0003] However, the multi-function paste of antistatic agents is not added, the volume resistance is up to 10 14 Ω ~ 10 17 Ω.cm, easy to generate charge accumulation, causing electrostatic dust, discharge, breakdown, severe...

Claims

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Application Information

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IPC IPC(8): C08L27/06C08L67/00C08K3/04C08K5/12C08K5/11H05K9/00
CPCC08L27/06H05K9/0081C08L2201/04C08K2201/011C08K2201/017C08K2201/001C08L67/00C08K3/041C08K5/12C08K5/11
Inventor 彭小权陈名海王小斌石红义
Owner JIANGXI COPPER TECHNOLOGY RESEARCH INSTITUTE CO LTD
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