Electrochemical polishing method capable of realizing single-phase solid solution high-entropy alloy
A high-entropy alloy and electrochemical technology, applied in the field of electrochemistry, can solve the problems of lack of systematicness and guidance, and achieve the effect of huge application potential
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[0031] 1) Weigh the Mo blocks, Co blocks, Cr blocks, Fe blocks, and Ni blocks with a purity of 99.99%, wash them and then melt and solidify them in an electric arc furnace to prepare FeCoCrNiMo with different Mo contents. X Alloys (x=0, 0.1, 0.3) are finally cut into round bars of Φ3×3.7mm, which are recorded as samples Mo0, Mo0.1, and Mo0.3.
[0032] 2) Use 1500-mesh sandpaper to grind off the cut marks on the round bar obtained in step 1) and clean it, and then put all the test materials such as pyrophyllite in a blast drying oven to dry for later use.
[0033] 3) Take two samples of Mo0.3 after drying in step 2), and pressurize them to 4GPa and 7GPa respectively in a high-temperature and high-pressure press at a temperature of 1700°C to obtain samples 4GPaMo0.3 and 7GPaMo0.3.
[0034] 4) According to the volume ratio of perchloric acid: alcohol = 1:15, configure the polishing agent.
[0035] 5) Take the samples Mo0, Mo0.1, Mo0.3, 4GPaMo0.3 and 7GPaMo0.3 and immerse them in...
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