Bio-based all-fiber self-powered multifunctional electronic skin and preparation method thereof
An electronic skin, self-powered technology, applied in the direction of fiber chemical characteristics, conductive/antistatic filament manufacturing, conjugated synthetic polymer artificial filament, etc., can solve the problem of incomplete use of multifunctional electronic skin, complicated production process, expensive Manufacturing and other issues, to achieve the effect of humidity and temperature sensitivity and good detection range, high air permeability, excellent pressure
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[0065] Example one
[0066] (1) Preparation of polyvinyl alcohol / polyvinylfluoroethylene negative friction layer: polyvinyl alcohol dissolves in deionized water at 80 ° C, stirring 3 h, and concentration of 18 wt%. 1 wt% of polyvinylidene fluoride powder was added, and 10 h was stirred, and the uniform dispersion of 19 wt% polyvinyl alcohol / polyvinylidene alcohol / polyvinylidene. The copper net is fixed to the collector of the needle 10 cm, and is uniformly covered by polyvinyl alcohol / polyvinylidene fluoride nanofibers. The electrospinning machine is maintained under certain spinning conditions during the working process, and the feed rate is 1 ml h. –1 . Finally, the sample was placed in an oven at 30 ° C for 6 h to remove the residual solvent.
[0067] (2) Preparation of collagen aggregate positive friction layer and assembly of self-generating pressure sensitive layers: 5 wt% collagen aggregate dissolved in hexafluoroprophane, stirred at 30 ° C for 40 min. Electrostatic...
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[0071] Example 2
[0072] (1) Preparation of polyvinyl alcohol / polyvinyl fluoride negative friction layer: polyvinyl alcohol dissolves in deionized water at 90 ° C, stirred 5 h, and concentration of 9 wt%. 9 wt% polyvinylidene fluoride was added, stirred for 20 h, and 18 wt% of polyvinyl alcohol / polyvinylidene fluoride was prepared. The copper net is fixed to the collector of the needle 15 cm, and is uniformly covered by polyvinyl alcohol / polyvinylidene fluoride nanofibers. The electrospinning machine is maintained under certain spinning conditions during the working process, and the feed rate is 1.5 ml. –1 . Finally, the sample was placed in an oven of 50 ° C to dry 3 h to remove the residual solvent.
[0073] (2) Preparation of collagen aggregate positive friction layer and assembly of the generated pressure sensitive layer: 10 wt% collagen aggregate dissolved in hexafluoropropyl alcohol, stirred at 40 ° C for 30 min. Electrostatic spinning in a certain environmental condi...
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[0077] Example three
[0078] (1) Preparation of polyvinyl alcohol / polyvinyl fluoride negative friction layer: Polyvinyl alcohol dissolves in 100 ° C deionized water, stirring 1 h, and concentration of 1 wt%. Further, 17 wt% polyvinylidene fluoride powder was added, stirred from 10 to 30 h, and the uniform dispersion of 18 wt% polyvinyl alcohol / polyvinylidene fluoride was prepared. The copper web is fixed to the collector of the needle 20 cm, and is uniformly covered by polyvinyl alcohol / polyvinylidene fluoride nanofibers. Electrostatic spinning machine remains in a certain spinning condition during operation, the feed rate is 2 ml ∙ h –1 . Finally, the sample was placed in an oven at 70 ° C for 1 h to remove the residual solvent.
[0079] (2) Preparation of collagen aggregate positive friction layer and assembly of the generated pressure sensitive layer: 18 wt% collagen aggregate dissolved in hexafluoropropyl alcohol, stirred at 50 ° C for 10 min. Electrostatic spinning in ...
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