Preparation method of antibacterial and anti-yellowing regenerated cellulose fabric
A technology of regenerated cellulose and fabrics, applied in fiber treatment, plant fibers, dyeing methods, etc., can solve the problems of non-environmental protection, anti-yellowing, poor antibacterial effect of anti-yellowing fabrics, achieve good anti-yellowing performance, increase smoothness, Enhance the effect of bond fastness
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[0034] Example 1
[0035] (1) Prior to viscose fiber yarns: Immersion regenerated cellulose fabric in the pretreatment solution, the concentration of each component in the treatment liquid is: pure base 2g / L, penetrant JFC 0.5 g / L, water resonance Among them, the temperature is 70 ° C, the time is 10 min;
[0036] (2) Preparation of anti-yellow yarn, anti-yellow finishing agent (phenolic oxidant, phosphite mass ratio 6: 1, polyether emulsifier quality is 0.2% of the mass of anti-yellow finishing agent) Dosage is 3% , PH = 5.0 (adjusted by acetic acid or citric acid), the bath ratio of 1: 40, 60 ° C for 3 h, washed repeatedly with deionized water, and the modified yarn of the anti-yellow finishing agent was obtained.
[0037](3) Preparation of antibacterial yarn: Precursted yarns placed in cyclodextrin and citric acid solution (cyclodextrin concentration of 40 g / L, crosslinking agent citric acid is 25 g / L), temperature rise to 80 After the treatment was 60 min, the β-CD / y...
Example Embodiment
[0042] Example 2
[0043] (1) Treatment of Mordale Fiber Yar: Immersion the regenerated cellulose fabric in the previous treatment solution, the concentration of each component in the treatment liquid is: pure base 2g / L, penetrant JFC 0.5 g / L, water rate; The temperature is 70 ° C, the time is 10 min;
[0044] (2) Preparation of anti-yellow yarn, the anti-yellow finishing agent (same as in Example 1) is 3%, pH = 5.0 (adjusted by acetic acid or citric acid), the bath ratio is 1: 30, 60 ° C for 3 h, Deion water is repeatedly cleaned and dried to obtain a yarn to modify the anti-yellow finishing agent;
[0045] (3) Preparation of antibacterial yarn: Precursted yarns placed in cyclodextrin and citric acid solution (cyclodextrin concentration of 40 g / L, crosslinking agent citric acid is 25 g / L), temperature rise to 80 After the treatment was 60 min, the β-CD / yarn was obtained after washing. The modified fibers were placed in a copper sulfate solution of 10 g / L, and the bath...
Example Embodiment
[0050] Example 3
[0051] (1) Temperature treatment: Immersion of the regenerated cellulose fabric in the pretreatment solution, the concentration of each component in the treatment liquid is: pure base 2 g / L, penetrant JFC 0.5 g / L, water rate; Among them, the temperature is 70 ° C, the time is 10 min;
[0052] (2) Preparation of anti-yellow yarn, the anti-yellow finishing agent (same as in Example 1) is 3%, pH = 5.0 (adjusted by acetic acid or citric acid), the bath ratio is 1: 30, 60 ° C for 3 h, Deion water is repeatedly cleaned and dried to obtain a yarn to modify the anti-yellow finishing agent;
[0053] (3) Preparation of antibacterial yarn: Precursted yarns placed in cyclodextrin and citric acid solution (cyclodextrin concentration of 40 g / L, crosslinking agent citric acid is 25 g / L), temperature rise to 80 After the treatment was 60 min, the β-CD / yarn was obtained after washing. The modified yarn was placed in a copper sulfate solution of 10 g / L, and the bath r...
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