Ketulao extract as well as preparation method and application thereof
A technology of cough dilo extract and cough dilo, which is applied in the field of cough dilo extract and its preparation, can solve the problems of insufficient aroma and purity, low sensory quality level, and low product quality, so as to achieve rich aroma and taste, High content of volatile small molecules, avoiding the effect of sticky core
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[0027] The embodiment of the present invention provides a preparation method of cough dill extract, comprising the following steps:
[0028] S01: Provide the raw material kedi, after selection, removal of impurities, and crushing, the kedi shreds are obtained;
[0029] S02: Subcritical extraction is performed on the kedilo crushed material to obtain a kedilo extract;
[0030] S03: Add the crude essential oil of the Kedilo extract into molecular distillation equipment, adjust the distillation temperature of the molecular distillation equipment to 10-100°C, the condensation temperature to 0-20°C, the pressure to 1-100Pa, and the rotation speed to 200 -300r / min, carry out molecular distillation separation and purification to obtain light components and heavy components, and collect the light components to obtain the essence of Kediguo.
[0031] Specifically, in the above step S01, the cough dill can be purchased from the market, or can be prepared and obtained by oneself. Speci...
Embodiment 1
[0041] A cough dill extract, the preparation method of which comprises the following steps:
[0042] S01: Provide the raw material Kedilo, select, remove impurities, remove cores, and pulverize to obtain Kedilo scraps, and the particle size of the Kedilo scraps is 100 mesh;
[0043] S02: Subcritical extraction is carried out on the scraped Kedilo. The temperature of the subcritical extraction is 40°C, and the extraction time is 1.5 hours. The liquid part obtains the crude extract of Kedilao, and the subcritical extraction is realized by subcritical fluid and entrainer co-processing, and the subcritical fluid is a mixture of propane, butane, and dimethyl ether, and the ratio of the three gases is 2:2:1, the entraining agent is a mixture of ethanol and propylene glycol, the weight ratio of the two entraining agents is 2:1, and the amount of the entraining agent accounts for 10% of the total weight of the cough dill scraps %;
[0044] S03: Add the Kedilo extract to molecular di...
Embodiment 2
[0046] A cough dill extract, the preparation method of which comprises the following steps:
[0047] S01: Provide the raw material Kedilo, select, remove impurities, remove cores, and pulverize to obtain Kedilo scraps, and the particle size of the Kedilo scraps is 100 mesh;
[0048] S02: Subcritical extraction is carried out on the Kedilo fragments, the temperature of the subcritical extraction is 30°C, and the extraction time is 2 hours. After the subcritical extraction is completed, the pressure of the equipment is adjusted to separate the gas and liquid, and the collected The liquid part obtains the crude extract of Kedilao, and the subcritical extraction is realized by subcritical fluid and entrainer co-processing, and the subcritical fluid is a mixture of propane, butane, and dimethyl ether, and the ratio of the three gases is 2:2:1, the entraining agent is a mixture of ethanol, propylene glycol, and glycerin, the weight ratio of the three entraining agents is 1:1:1, and ...
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