Method for making ammonium polyphosphate clad by microcapsules
A technology of coating ammonium polyphosphate and ammonium polyphosphate, applied in the direction of microcapsule preparation, microsphere preparation, etc., can solve the problems of long-term contact with water, environmental pollution, and reduced yield of coated APP, etc.
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[0036] Example 1
[0037] In a reactor equipped with a stirring and reflux device, add 180ml of ethanol and 100g of APP, heat to 80°C under stirring, then add 28g of melamine-formaldehyde prepolymer, and then add ammonium chloride of 2.0% by weight of the prepolymer. Stir and react for about 30 minutes to harden the resin. Then lower the temperature of the kettle to about 50°C, add 1.0% urea equivalent to the weight of the solid reactant, continue to stir and react for about 30 minutes, cool, filter, and dry the filter cake at 90°C and 30mmHg to obtain good free flow. The coated APP is 115.5g.
Example Embodiment
[0038] Example 2
[0039] In a reactor equipped with a stirring and reflux device, add 180ml of ethanol and 100g of APP, and add 35g of melamine-formaldehyde prepolymer at a temperature of 80°C, and add 3.0% ammonium chloride by weight of the prepolymer, stir, React for 60 minutes to harden the resin. Then lower the temperature of the kettle to about 50°C, then add 3.0% urea equivalent to the weight of the solid reactant, continue to stir and react for about 20 minutes, cool and filter, and dry the filter cake at 90°C and 30mmHg to obtain good fluidity. White coated APP 112.6g.
Example Embodiment
[0040] Example 3
[0041]The feeding and operation are carried out according to Example 1, but the addition amount of prepolymer is 17g, the addition amount of ammonium chloride is 2% of the weight of the prepolymer, and the addition amount of urea is 1% of the weight of the solid reactant, and the reaction is complete. After that, it was cooled and filtered, and the filter cake was dried at 90° C. and 30 mmHg to obtain 105.8 g of white coated APP with good free-flowing properties.
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