Value document
A technology for valuable documents and parts, applied in the field of valuable documents, which can solve problems such as obstructing identification
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example 1
[0123] To prepare the starting material for oxidative formation, the material that can be converted to an oxide is mixed with the chromophore in appropriate proportions according to formula (1), and then annealed, crushed, washed (eg, with water), dried and ground. The color base used can be Mn 2 o 3 , MnO, MnO 2 , MnCo 3 , MnCl 2 , KMnO 4 and organomanganese compounds. The weight fraction of color bases, based on the total mixture, can be up to 20% by weight. The annealing is carried out in the temperature range of 200-1700°C, and the holding time is 0.2-24 hours, but preferably at 300-500°C, and the holding time is 0.5-2 hours.
[0124] (1)6LiOH+As 2 o 5 +xMNCl 2 ? 2Li 3 AsO 4 :Mn+3H 2 O+xCl 2
[0125] In order to shift the equilibrium state in the direction of product formation, it can additionally be mixed with preferably 1-5% by weight of LiCO 3 Mixing, and additionally mixing with preferably 1-20% by weight LiOH for preparation.
example 2
[0127] Appropriate amount of sulfate (such as K 2 SO 4 ), or chromates (such as K 2 CrO 4 ) and an appropriate amount of dopant (such as Na 2 FeO 4 ) dissolved in alkaline medium. With up to 20% Na 2 FeO 4 doping. Evaporation of the solvent gave the product, which was ground for further use.
[0128] In addition, solid-state reactions can also be carried out. For this purpose, the K 2 SO 4 Grind with NaCl, and with Fe 3 o 4 Mix well. The mixture is annealed at a temperature of 700-1800°C. The product is reground for further use.
example 3
[0130] A variation of the procedure described in Example 2 was used to evaporate the solvent using a spray dryer. Alternatively, the alkaline medium may consist completely or partly of a silicate suspension (eg LUDOX AS-40, DuPont). In this case, a silicate-encapsulated material is obtained after spray drying. Then an annealing process is performed at a temperature of 200-600 ° C to form SiO 2 protective layer and stabilizes the solubility of the substance in water. Alternatively, the material can be embedded in a polymer such as PMMA and processed into a foil material. The foil material is then cut into discs.
[0131] Other embodiments and advantages of the present invention can be referred to figure 2 Be explained.
[0132] figure 2 Represents a cross-section of a security element according to the invention.
[0133] figure 2 An embodiment of the security element of the present invention is represented. In this case, the security element consists of a label 2...
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