Engineering plastic resin compsn. able to be low temp decomposed and method of producing molding using the same
A technology of resin composition and engineering plastics, applied in the field of engineering plastics resin composition
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[0097] The following examples are intended to further describe the present invention in detail, but should by no means be construed as limiting the scope of the present invention. It should also be understood that the formulation amount (% by mass) of the fluorine-containing resin is based on the total amount of the combined fluorine-containing resin and low-temperature decomposable engineering plastics.
Synthetic example -1
[0099] Synthesis of Fluorine Resin
[0100] Put 200L of pure water into an 820L glass-lined autoclave, and then vacuumize after bubbling thoroughly with nitrogen. Charge 113 kg 1-fluoro-1,1-dichloroethane, 95 kg hexafluoropropene (HFP) and 85 kg cyclohexane, charge 292 g perfluoro(1,1,5-trihydro-1-pentane ene) (HF-Pe), and the system was maintained at 35° C. and a stirring speed of 200 rpm. After that, load tetrafluoroethylene (TFE) until it reaches 0.71MPaG (7.25kg / cm 2 G), then charge ethylene until it reaches 0.78MPaG (8kg / cm 2 G).
[0101] A solution of di-n-propylperoxydicarbonate in methanol (50%, 1.9 kg) was charged to initiate polymerization. A mixed gas of TFE:ethylene (Et):HFP (39.2:43.6:17.3 mole%) was continuously supplied to the system so as to keep the inner pressure of the autoclave at 0.78 MPaG. Stirring was continued for 32 hours while continuing to supplement perfluoro(1,1,5-trihydro-1-pentene). The system pressure was returned to atmospheric pressure, ...
Embodiment 1
[0109] The fluorine-containing resin obtained by Synthesis Example-1 is formulated with polyacetal (product name: Derlin 150SA, produced by E.I.du Pont de Nemours and Company) in a ratio of 0.25% by mass, and these materials are blended in polyethylene bags, And using an extrusion film molding machine (type: single shaft; screw size: 30mm, LD: 25; round rod die: 30mm, L330mm; manufactured by Rikua) at a screw rotation speed of 6-7rpm and an extrusion temperature of 200°C molded. Extrusion torque, extrusion pressure and extrusion speed are shown in Table 1.
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