Resin composition and process for producing molding
A technology of resin composition and production method, which is applied in the field of resin composition, and can solve the problems of not adding perfluoropolymer perfluoropolymer publicly
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preparation example Construction
[0065] The preparation method of the resin composition of the present invention is not particularly limited, but includes hitherto known methods. A typical method includes preparing the fluorine-containing resin and the engineering plastics in the above-mentioned preparation ratio, and melt-kneading the resulting mixture under selective heating conditions, and the preparation process can optionally add other components .
[0066] In the compounding step, the other components may be blended with the fluorine-containing resin and / or the engineering plastic in advance, or the other components.
[0067] At the latest when the resin composition is molded, the above-mentioned fluorine-containing resin and engineering plastic should be present in a ratio within the above-mentioned range. Therefore, the formulation method includes, but is not limited to, a method including blending the fluorine-containing resin and engineering plastics at a ratio within the above-mentioned range fro...
Embodiment
[0104] The following examples are intended to further describe the present invention in detail, but should by no means be construed as limiting the scope of the present invention. It should also be understood that the formulation amount (% by mass) of the fluorine-containing resin is based on the total amount of the fluorine-containing resin and engineering plastics.
Synthetic example -1
[0106] Synthesis of FEP Copolymer
[0107] In a 1000 L glass-lined vertical autoclave equipped with a stirrer, 200 kg of pure water and 0.1 kg of ω-hydroxyl fluorocarboxylate ammonium were charged, and nitrogen replacement and vacuum degassing were carried out three times. Then, 233 kg of hexafluoropropylene (HFP) and 2.3 kg of perfluoro(propyl vinyl ether) (PPVE) were charged in the autoclave under vacuum.
[0108]Stirring was started and the temperature of the polymerization vessel was set to 29.0°C. Then, tetrafluoroethylene (TFE) was introduced to increase the pressure to 0.9 MPaG. Then 3.8 kg of di(ω-hydrodecafluoroheptanoyl) peroxide (DHP) diluted to about 8 wt% with perfluorohexane was charged into the autoclave, and the reaction started immediately after the addition.
[0109] During this reaction, TFE was supplemented to the system and the inner pressure of the autoclave was maintained at 0.9 MPaG. After 9, 18 and 27 hours of reaction, additional 0.5 kg portions of...
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